1,4-二(十二烷氧基)苯合成路线 （共 13 条）
反应条件
KIO3; sulfuric acid; iodine in acetic acid T=120°C;
参考文献
Gonzalez-Rojano, Norma; Arias-Marin, Eduardo; Navarro-Rodriguez, Damaso; Weidner, Steffen
Synlett, 2005 , # 8 art. no. S01505ST, p. 1259 - 1262
反应条件
1: 61 percent / HBr / acetic acid / 2 h / 70 - 75 °C
2: 51 percent / dimethylformamide / 48 h / 110 °C
View Scheme
参考文献
Thompson, Barry C.; Kim, Young-Gi; McCarley, Tracy D.; Reynolds, John R.
Journal of the American Chemical Society, 2006 , vol. 128, # 39 p. 12714 - 12725
反应条件
1: mercury(II) diacetate; iodine / dichloromethane / 12 h / 20 °C
2: copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); triethylamine / tetrahydrofuran / 12 h / 20 °C / Inert atmosphere
View Scheme
参考文献
Llanes-Pallas, Anna; Yoosaf; Traboulsi, Hassan; Mohanraj, John; Seldrum, Thomas; Dumont, Jacques; Minoia, Andrea; Lazzaroni, Roberto; Armaroli, Nicola; Bonifazi, Davide
Journal of the American Chemical Society, 2011 , vol. 133, # 39 p. 15412 - 15424
