反应条件
1: sulfuric acid; potassium nitrate / 6 h / 0 - 60 °C / Inert atmosphere 2: manganese(IV) oxide / toluene / 2 h / Inert atmosphere; Reflux 3: palladium 10 on activated carbon; hydrogen / methanol / 3 h / 760.05 Torr 4: hydrogen bromide; copper(I) bromide; sodium nitrite / water / 12.5 h / 0 - 75 °C / Inert atmosphere View Scheme
参考文献
Shi, Jun; Manolikakes, Georg; Yeh, Chien-Hung; Guerrero, Carlos A.; Shenvi, Ryan A.; Shigehisa, Hiroki; Baran, Phil S.
Journal of the American Chemical Society, 2011 , vol. 133, # 20 p. 8014 - 8027