magnesium in toluene byproducts: MgBrCl; (Ar); treatment of o-BrC6H4OCH3 with Mg in toluene; reflux with GeCl4 for 30 h; treatment with satd. aq. NH4Cl; extn. of aq. layer with THF; drying of combined extracts over MgSO4; removal of THF (vac.); recrystn. twice fromEtOH or MeCN; elem. anal.;
参考文献
Yoder, Claude H.; Agee, Tamara M.; Griffith, Allison K.; Schaeffer Jr., Charles D.; Carroll, Mary J.; Detoma, Alaina S.; Fleisher, Adam J.; Gettel, Cameron J.; Rheingold, Arnold L.
Organometallics, 2010 , vol. 29, # 3 p. 582 - 590
