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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
3233-06-5
合成路线
（共 21 条）
74497-02-2
+
75-56-9
环氧丙烷
→
反应条件
16955-09-2
+
3233-06-5
反应条件
CF3O3S(1-)*C14H14BiO3(1+) in water T=20°C; 6 h; regioselective reaction;
参考文献
Tan, Nianyuan; Yin, Shuangfeng; Li, Yuefang; Qiu, Renhua; Meng, Zhengong; Song, Xingxing; Luo, Shenglian; Au, Chak-Tong; Wong, Wai-Yeung
Journal of Organometallic Chemistry, 2011 , vol. 696, # 8 p. 1579 - 1583
74497-02-2
+
75-56-9
环氧丙烷
→
反应条件
3233-06-5
反应条件
zirconium tetrachloride T=20°C; 0.25 h;
参考文献
Chakraborti, Asit K.; Kondaskar, Atul; Rudrawar, Santosh
Tetrahedron, 2004 , vol. 60, # 41 p. 9085 - 9091
74497-02-2
+
75-56-9
环氧丙烷
→
反应条件
3233-06-5
+
3077-13-2
1,1’-(苯基亚氨基)双-2-丙醇
反应条件
zinc(II) bis(tetrafluoroborate) hydrate T=20°C; 0.333333 h; Inert atmosphereNeat (no solvent);
参考文献
Pujala, Brahmam; Rana, Shivani; Chakraborti, Asit K.
Journal of Organic Chemistry, 2011 , vol. 76, # 21 p. 8768 - 8780
108-86-1
溴代苯
+
78-96-6
异丙醇胺
→
反应条件
3233-06-5
反应条件
copper(l) chloride; potassium hydroxide T=90°C; 8 h; Neat (no solvent);
参考文献
Yin, Huiqing; Jin, Ming; Chen, Wei; Chen, Chen; Zheng, Likang; Wei, Ping; Han, Shiqing
Tetrahedron Letters, 2012 , vol. 53, # 10 p. 1265 - 1270
591-50-4
碘苯
+
78-96-6
异丙醇胺
→
反应条件
3233-06-5
反应条件
copper(l) chloride; potassium hydroxide T=20°C; 8 h; Neat (no solvent);
参考文献
Yin, Huiqing; Jin, Ming; Chen, Wei; Chen, Chen; Zheng, Likang; Wei, Ping; Han, Shiqing
Tetrahedron Letters, 2012 , vol. 53, # 10 p. 1265 - 1270
74497-02-2
+
127-00-4
氯丙醇
→
反应条件
3233-06-5
反应条件
sodium hydrogencarbonate in acetonitrile T=100°C; 24 h;
参考文献
Cho, Chan Sik; Kim, Jin Hwang; Kim, Tae-Jeong; Shim, Sang Chul
Tetrahedron, 2001 , vol. 57, # 16 p. 3321 - 3329
996-21-4
+
74497-02-2
→
反应条件
3233-06-5
+
3077-13-2
1,1’-(苯基亚氨基)双-2-丙醇
反应条件
triethylamine in methanol 4 h; Reflux;
参考文献
Sechi, Mario; Rizzi, Giuseppe; Bacchi, Alessia; Carcelli, Mauro; Rogolino, Dominga; Pala, Nicolino; Sanchez, Tino W.; Taheri, Laleh; Dayam, Raveendra; Neamati, Nouri
Bioorganic and Medicinal Chemistry, 2009 , vol. 17, # 7 p. 2925 - 2935
108-32-7
碳酸丙烯酯
+
74497-02-2
→
反应条件
109605-09-6
+
16955-09-2
+
3233-06-5
+
1258887-18-1
+
3077-13-2
1,1’-(苯基亚氨基)双-2-丙醇
+
129118-34-9
反应条件
[(n-Oct)3MeP][Br] T=170°C; 40 h; Ionic liquidNeat (no solvent);
参考文献
Selva, Maurizio; Fabris, Massimo; Lucchini, Vittorio; Perosa, Alvise; Noe, Marco
Organic and Biomolecular Chemistry, 2010 , vol. 8, # 22 p. 5187 - 5198
187737-37-7
+
74497-02-2
→
反应条件
16955-09-2
+
3233-06-5
反应条件
tetrafluoroboric acid; water; mercury(II) oxide 1.) THF, -10 deg C, 5 min, 2.) reflux, 6 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Barluenga, Jose; Alonso-Cires, Luisa; Asensio, Gregorio
Synthesis, 1981 , # 5 p. 376 - 378
13746-81-1
→
反应条件
3233-06-5
反应条件
perchloric acid in 1,4-dioxane T=10°C; Kinetics; Further Variations:Reagents;
参考文献
Kutuk, Halil; Bekdemir, Yunus; Turkoz, Nalan
Phosphorus, Sulfur and Silicon and the Related Elements, 2006 , vol. 181, # 4 p. 931 - 937
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