反式-1,4-环已烷二甲醇合成路线 （共 20 条）
反应条件
C16H30O; MCHM T=225°C; P=258581 Torr;
参考文献
WO2013/19441 A1, ;
Paragraph 0118 ;
反应条件
hydrogen; AlO(OH); rhodium in ethyl acetate T=22°C; P=760 Torr; 46 h; Title compound not separated from byproducts;
参考文献
Chemical Communications, , # 45 p. 5667 - 5669
反应条件
CrO4(2-)*Ba(2+)*Cr2CuO4*CuO; hydrogen T=250°C; P=212036 Torr; 5 h; PressureTemperature;
参考文献
WO2013/19439 A1, ;
Paragraph 0102 ;
反应条件
lithium aluminium tetrahydride in diethyl ether T=20°C; Reduction;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 71, # 7 p. 1639 - 1647
反应条件
(Py)Zn(BH4)2 in tetrahydrofuran 0.4 h; Heating;
参考文献
Journal of Chemical Research - Part S, , # 8 p. 522 - 525
反应条件
in tetrahydrofuran; (2S)-N-methyl-1-phenylpropan-2-amine hydrate
反应条件
potassium carbonate Ambient temperature;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 43, # 3 p. 529 - 531
反应条件
in acetone 168 h; Ambient temperaturelipase PS (Pseudomonas sp.) on Celite; Yields of byproduct given;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 43, # 3 p. 529 - 531
反应条件
1: 6 h / 260 - 280 °C / 4535.33 Torr 2: cyclohexane-1,4-dicarboxylic acid dimethyl ester; Pd/Al2O3; hydrogen / 1 h / 200 °C / 93849.2 Torr / |Autoclave 3: C16H30O; MCHM / 225 °C / 258581 Torr View Scheme
反应条件
1: 52.1 percent / 140 - 165 °C 2: 46.3 percent / aq. NaOH / 10 h / Heating View Scheme
参考文献
Physical Chemistry Chemical Physics, , vol. 6, # 15 p. 3977 - 3984
