反应条件
1.1: AlCl3, aluminium chloride / acetonitrile / 0 °C / |Reflux 1.2: |Cooling with ice 2.1: sodium tetrahydroborate / ethanol / 0 - 20 °C 3.1: Lux cellulose-1 PHENOMENIX column / acetonitrile; water / |Resolution of racemate View Scheme
参考文献
Goel, Atul; Kumar, Amit; Hemberger, Yasmin; Raghuvanshi, Ashutosh; Jeet, Ram; Tiwari, Govind; Knauer, Michael; Kureel, Jyoti; Singh, Anuj K.; Gautam, Abnish; Trivedi, Ritu; Singh, Divya; Bringmann, Gerhard
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 48 p. 9583 - 9592
