E-6,10-二甲基-5,9-十一碳二烯-2-醇乙酸酯合成路线 （共 12 条）
反应条件
4-(N,N-dimethlyamino)pyridine in pyridine T=0°C; 0.5 h;
参考文献
Li, Ying; Lu, Biao; Li, Chunhong; Li, Yulin
Synthetic Communications, 2003 , vol. 33, # 8 p. 1417 - 1423
反应条件
trifluoroacetic acid in nitromethane T=0°C; 1.5 h; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Tetrahedron, , vol. 44, p. 2913
反应条件
1: POCl3 / pyridine / 15 h / Ambient temperature 2: TFA / nitromethane / 1.5 h / 0 °C View Scheme
参考文献
Tetrahedron, , vol. 44, p. 2913
反应条件
1: 8 percent Chromat. / KHSO4 / 0.75 h / 140 °C / investigation of regioselectivity of dehydration with var. reagents in terpene derivatives 2: TFA / nitromethane / 1.5 h / 0 °C 3: POCl3 / pyridine / 15 h / Ambient temperature View Scheme
参考文献
Tetrahedron, , vol. 44, p. 2913
反应条件
1: TFA / nitromethane / 1.5 h / 0 °C 2: POCl3 / pyridine / 15 h / Ambient temperature View Scheme
参考文献
Tetrahedron, , vol. 44, p. 2913
反应条件
2: 89 percent / pyridine 3: POCl3 / pyridine / 15 h / Ambient temperature View Scheme
参考文献
Tetrahedron, , vol. 44, p. 2913
反应条件
2: 89 percent / pyridine 3: POCl3 / pyridine / 15 h / Ambient temperature View Scheme
参考文献
Tetrahedron, , vol. 44, p. 2913
反应条件
1: TFA / nitromethane / 1.5 h / 0 °C 2: POCl3 / pyridine / 15 h / Ambient temperature View Scheme
参考文献
Tetrahedron, , vol. 44, p. 2913
反应条件
1: 89 percent / pyridine 2: POCl3 / pyridine / 15 h / Ambient temperature View Scheme
参考文献
Tetrahedron, , vol. 44, p. 2913
反应条件
1: 98 percent / sodium borohydride / methanol / 0.5 h / 0 °C 2: 100 percent / DMAP / pyridine / 0.5 h / 0 °C View Scheme
参考文献
Synthetic Communications, , vol. 33, # 8 p. 1417 - 1423
