5-甲基-5-己烯-2-酮合成路线 （共 36 条）
反应条件
1: aluminium isopropylate; isopropyl alcohol
3: acetic acid; sulfuric acid / beim Erwaermen des Reaktionsprodukts mit wss. Natronlauge
View Scheme
参考文献
La Forge et al.
Journal of Organic Chemistry, 1952 , vol. 17, p. 457,465
反应条件
sulfuric acid
1 h; Title compound not separated from byproducts;
参考文献
Bates, Hans Aaron
Journal of the American Chemical Society, 1982 , vol. 104, # 9 p. 2490 - 2493
反应条件
sodium tetrahydroborate
参考文献
Ashcroft, Martyn M.; Bougeard, Peter; Bury, Adrian; Cooksey, Christopher J.; Johnson, Michael D.; et al.
Journal of Organic Chemistry, 1984 , vol. 49, # 10 p. 1751 - 1761
反应条件
hydrogen; carbon monoxide in cyclohexane
T=20 - 25°C; P=760 - 798 Torr; 1 h; other catalyst; Product distribution;
参考文献
Ishiyama, Jun-ichi; Maeda, Satoshi; Takahashi, Kazuhiro; Senda, Yasuhisa; Imaizumi, Shin
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 5 p. 1721 - 1726
反应条件
1: diethyl ether
2: palladium/calcium carbonate; ethyl acetate / Hydrogenation.Behandlung der Reaktionsloesung mit wss.Salzsaeure
View Scheme
参考文献
Arens; Modderman
Pr.Akad.Amsterdam<B>, 1951 , vol. 54, p. 236,238
反应条件
sodium hydride in diethyl ether
参考文献
Leyendecker,F.
Tetrahedron, 1976 , vol. 32, p. 349 - 353
