1-苯基-4-戊烯-1-酮合成路线 (共 116 条)
反应条件
NOBF4 in acetonitrile T=-23°C; Oxidation;
参考文献
Tetrahedron Letters, , vol. 40, # 37 p. 6773 - 6776
反应条件
water; oxygen; copper diacetate; palladium dichloride in N,N-dimethyl acetamide T=20°C; 48 h;
参考文献
Paradas, Miguel; Campana, Araceli G.; Estevez, Rosa E.; De Cienfuegos, Luis Alvarez; Jimenez, Tania; Robles, Rafael; Cuerva, Juan M.; Oltra, J. Enrique
Journal of Organic Chemistry, 2009 , vol. 74, # 9 p. 3616 - 3619
反应条件
1: acetophenone With potassium hydride in tetrahydrofuran
T=23°C; 0.5 h;
2: allyl bromide With triethyl borane in tetrahydrofuran
T=23°C; 4 h;
参考文献
Waser, Jerome; Gaspar, Boris; Nambu, Hisanori; Carreira, Erick M.
Journal of the American Chemical Society, 2006 , vol. 128, # 35 p. 11693 - 11712
反应条件
dipyridinium dichromate in dichloromethane
T=20°C; 12 h;
参考文献
Zhu, Jia-Liang; Chan, Yu-Hui
Synlett, 2008 , # 8 p. 1250 - 1254
反应条件
potassium hydroxide; sodium in ethanol; water
参考文献
PHILLIPS PETROLEUM COMPANY
Patent: US2003/92925 A1, 2003 ;
反应条件
copper(l) chloride in tetrahydrofuran
T=40°C; 16 h;
参考文献
Yasuda, Makoto; Tsuji, Shoki; Shigeyoshi, Yusuke; Baba, Akio
Journal of the American Chemical Society, 2002 , vol. 124, # 25 p. 7440 - 7447
反应条件
copper(l) iodide in tetrahydrofuran
T=-10 - 20°C;
参考文献
Gribkov, Denis V.; Hultzsch, Kai C.; Hampel, Frank
Journal of the American Chemical Society, 2006 , vol. 128, # 11 p. 3748 - 3759
反应条件
lithium bromide in water; N,N-dimethyl-formamide
T=195 - 200°C; 72 h;
参考文献
Hok, Saphon; Schore, Neil E.
Journal of Organic Chemistry, 2006 , vol. 71, # 4 p. 1736 - 1738
反应条件
HEH; Ru(bpy)3Cl2 in pyridine
Ambient temperatureIrradiation;
参考文献
Liu, Qiang; Han, Bing; Liu, Zhengang; Yang, Li; Liu, Zhong-Li; Yu, Wei
Tetrahedron Letters, 2006 , vol. 47, # 11 p. 1805 - 1807
反应条件
bis(1,5-cyclooctadiene)nickel (0); para-fluorostyrene; pyphos in tetrahydrofuran
T=23°C; 0.166667 h;
参考文献
Zhang, Yongda; Rovis, Tomislav
Journal of the American Chemical Society, 2004 , vol. 126, # 49 p. 15964 - 15965