1-苯基-4-戊烯-1-酮合成路线 （共 116 条）
反应条件
sulfuric acid; mercuric sulphate
参考文献
Farbenfabr. Bayer
Patent: US2884464 , 1955 ;
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Farbenfabr. Bayer
Patent: DE1007767 , 1954 ;
反应条件
sodium methylate
Irradiation;
参考文献
Ojima,I.; Kondo,K.
Bulletin of the Chemical Society of Japan, 1973 , vol. 46, # 5 p. 1539 - 1545
反应条件
1: CuCl
2: aqueous methanol. H2SO4; HgSO4
View Scheme
参考文献
Farbenfabr. Bayer
Patent: US2884464 , 1955 ;
Full Text Show Details
Farbenfabr. Bayer
Patent: DE1007767 , 1954 ;
反应条件
lithium aluminium tetrahydride; n-butyllithium
1) THF, -78 deg C, 1 h, 2) THF, -78 deg C -> -5 deg C, 30 min, 3) THF, -5 deg C -> room temperature, 30 min; Yield given. Multistep reaction;
参考文献
Jang, Won Bum; Shin, Won Suk; Hong, Jong Eun; Lee, Shi Yong; Oh, Dong Young
Synthetic Communications, 1997 , vol. 27, # 19 p. 3333 - 3339
反应条件
potassium fluoride; 2,2'-azo-bisisobutyronitrile
1.) C6H6, reflux, 3 h, 2.) Et2O, r.t.; Yield given. Multistep reaction;
参考文献
Dang, Hai-Shan; Roberts, Brian P.
Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 8 p. 769 - 775
参考文献
Ng, Kai S.; Alper, Howard
Journal of Organic Chemistry, 1981 , vol. 46, # 5 p. 1039 - 1041
参考文献
Hurd; Pollack
Journal of the American Chemical Society, 1938 , vol. 60, p. 1905,1910
反应条件
in benzene
44 h; Irradiation; Product distributionMechanismQuantum yield;
参考文献
Wagner, Peter J.; Liu, Kou-Chang; Noguchi, Y.
Journal of the American Chemical Society, 1981 , vol. 103, # 13 p. 3837 - 3841
反应条件
in acetonitrile
T=20°C; Dehydrogenation; Decomposition; 0.0833333 h; UV-irradiation; Product distribution; Further Variations:Solvents;
参考文献
Nakamura, Mitsunobu; Miki, Masamichi; Majima, Tetsuro
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 3 p. 415 - 420
参考文献
Cope; Hofmann; Hardy
Journal of the American Chemical Society, 1941 , vol. 63, p. 1855
