1-苯基-4-戊烯-1-酮合成路线 （共 116 条）
反应条件
1: PdCl2(PPh3)2; N,N,N',N'-tetra-methylnaphthalene-1,8-diamine / methanol / 24 h / 100 °C / 3750.38 Torr / Gas phase
2: 4-(N,N-dimethlyamino)pyridine / 72 h / 90 °C
3: allyl alcohol; triphenylphosphine; bis(dibenzylideneacetone)-palladium(0) / methanol / 0.75 h / 90 °C
View Scheme
参考文献
Giboulot, Steven; Liron, Frederic; Prestat, Guillaume; Wahl, Benoit; Sauthier, Mathieu; Castanet, Yves; Mortreux, Andre; Poli, Giovanni
Chemical Communications, 2012 , vol. 48, # 47 p. 5889 - 5891
反应条件
bis(dibenzylideneacetone)-palladium(0) in N,N-dimethyl-formamide
3 h; Ambient temperature;
参考文献
Inoue, Yoshio; Toyofuku, Masanori; Taguchi, Masaaki; Okada, Shin-ichi; Hashimoto, Harukichi
Bulletin of the Chemical Society of Japan, 1986 , vol. 59, # 3 p. 885 - 892
反应条件
1: 92 percent / diethyl ether
2: 1.) AIBN, 2.) aq. KF / 1.) C6H6, reflux, 3 h, 2.) Et2O, r.t.
View Scheme
参考文献
Dang, Hai-Shan; Roberts, Brian P.
Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 8 p. 769 - 775
反应条件
2: Erhitzen auf Siedetemperatur
View Scheme
参考文献
Hurd; Pollack
Journal of the American Chemical Society, 1938 , vol. 60, p. 1905,1910
反应条件
1: 4-(N,N-dimethlyamino)pyridine / 72 h / 90 °C
2: allyl alcohol; triphenylphosphine; bis(dibenzylideneacetone)-palladium(0) / methanol / 0.75 h / 90 °C
View Scheme
参考文献
Giboulot, Steven; Liron, Frederic; Prestat, Guillaume; Wahl, Benoit; Sauthier, Mathieu; Castanet, Yves; Mortreux, Andre; Poli, Giovanni
Chemical Communications, 2012 , vol. 48, # 47 p. 5889 - 5891
反应条件
in benzene
T=25°C; Irradiationtriplet decay rate; further solvents; MechanismQuantum yield;
参考文献
Wagner,P.J.; Lindstrom,M.J.; Sedon,J.H.
Journal of the American Chemical Society, 1981 , vol. 103, p. 3842
反应条件
in benzene
T=25°C; Irradiationtriplet decay rate; MechanismQuantum yield;
参考文献
Wagner,P.J.; Lindstrom,M.J.; Sedon,J.H.
Journal of the American Chemical Society, 1981 , vol. 103, p. 3842
反应条件
DCN in water; acetonitrile
Irradiation;
参考文献
Pandey, Ganesh; Sochanchingwung, R.
Journal of the Chemical Society, Chemical Communications, 1994 , # 17 p. 1945 - 1946
反应条件
in benzene
T=25°C; Irradiationtriplet decay rate; MechanismQuantum yield;
参考文献
Wagner,P.J.; Lindstrom,M.J.; Sedon,J.H.
Journal of the American Chemical Society, 1981 , vol. 103, p. 3842
反应条件
in benzene
T=25°C; Irradiation; Mechanism;
参考文献
Wagner,P.J.; Lindstrom,M.J.; Sedon,J.H.
Journal of the American Chemical Society, 1981 , vol. 103, p. 3842
