N-乙酰基 -3-(3,4,5-三氟苯基 )-d-丙氨酸合成路线 (共 4 条)
反应条件
sodium hydroxide; Aspergillus genus acylase; sodium acetate in water T=38°C; 48 h;
参考文献
Matsushima; Fujita; Okada; Shirasu; Nose; Shimohigashi
Bulletin of the Chemical Society of Japan, 2000 , vol. 73, # 11 p. 2531 - 2538
反应条件
1: Na; C2H5OH / 2 h / Heating 2: NaOH; HCl / methanol / 3 h / 40 °C 3: xylene / 2 h / 139 °C 4: NaOH; CH3COONa; Aspergillus genus acylase / H2O / 48 h / 38 °C View Scheme
参考文献
Matsushima; Fujita; Okada; Shirasu; Nose; Shimohigashi
Bulletin of the Chemical Society of Japan, 2000 , vol. 73, # 11 p. 2531 - 2538
反应条件
1: xylene / 2 h / 139 °C 2: NaOH; CH3COONa; Aspergillus genus acylase / H2O / 48 h / 38 °C View Scheme
参考文献
Matsushima; Fujita; Okada; Shirasu; Nose; Shimohigashi
Bulletin of the Chemical Society of Japan, 2000 , vol. 73, # 11 p. 2531 - 2538
反应条件
1: NaOH; HCl / methanol / 3 h / 40 °C 2: xylene / 2 h / 139 °C 3: NaOH; CH3COONa; Aspergillus genus acylase / H2O / 48 h / 38 °C View Scheme
参考文献
Matsushima; Fujita; Okada; Shirasu; Nose; Shimohigashi
Bulletin of the Chemical Society of Japan, 2000 , vol. 73, # 11 p. 2531 - 2538