N-(4-甲氧基苄基)-2-苯基乙胺合成路线 (共 10 条)
反应条件
1: With palladium on aluminium oxyhydroxide in n-heptane T=90°C; 12 h; Inert atmosphere; 2: With hydrogen in n-heptane T=25°C; P=760.051 Torr; 6 h;
参考文献
Kwon, Min Serk; Kim, Sungjin; Park, Sungho; Bosco, William; Chidrala, Ravi Kumar; Park, Jaiwook
Journal of Organic Chemistry, 2009 , vol. 74, # 7 p. 2877 - 2879
反应条件
phenyl silane; di-n-butyldichlorostannane in tetrahydrofuran T=100°C; 0.116667 h; microwave irradiation;
参考文献
Kangasmetsae, Jussi J.; Johnson, Tony
Organic Letters, 2005 , vol. 7, # 25 p. 5653 - 5655
反应条件
N,N,N',N,-tetramethylethylenediamine; lithium hexamethyldisilazane in benzene-d6 T=120°C; 1.9 h;
参考文献
Horrillo-Martinez, Patricia; Hultzsch, Kai C.; Gil, Adria; Branchadell, Vicenc
European Journal of Organic Chemistry, 2007 , # 20 p. 3311 - 3325
反应条件
sodium tetrahydroborate in methanol Yield given;
参考文献
Siegel, Miles G.; Hahn, Patric J.; Dressman, Bruce A.; Fritz, James E.; Grunwell, Jocelyn R.; Kaldor, Stephen W.
Tetrahedron Letters, 1997 , vol. 38, # 19 p. 3357 - 3360
反应条件
1: 99 percent / DEAD, PPh3 / benzene / 0.33 h / 23 °C 2: 97 percent / HSCH2COOH, Et3N / CH2Cl2 / 0.08 h / 23 °C View Scheme
参考文献
Fukuyama, Tohru; Cheung, Mui; Jow, Chung-Kuang; Hidai, Yuko; Kan, Toshiyuki
Tetrahedron Letters, 1997 , vol. 38, # 33 p. 5831 - 5834
反应条件
1: methanol 2: sodium borohydride / methanol View Scheme
参考文献
Siegel, Miles G.; Hahn, Patric J.; Dressman, Bruce A.; Fritz, James E.; Grunwell, Jocelyn R.; Kaldor, Stephen W.
Tetrahedron Letters, 1997 , vol. 38, # 19 p. 3357 - 3360
反应条件
1: methanol 2: sodium borohydride / methanol View Scheme
参考文献
Siegel, Miles G.; Hahn, Patric J.; Dressman, Bruce A.; Fritz, James E.; Grunwell, Jocelyn R.; Kaldor, Stephen W.
Tetrahedron Letters, 1997 , vol. 38, # 19 p. 3357 - 3360
反应条件
n-butyllithium in toluene T=40°C; 12 h;
参考文献
Hamana, Hiroshi; Iwasaki, Fuminori; Nagashima, Hiroyoshi; Hattori, Kazuhisa; Hagiwara, Tokio; Narita, Tadashi
Bulletin of the Chemical Society of Japan, 1992 , vol. 65, # 4 p. 1109 - 1113
反应条件
1: DIAD; polymer-bound triphenylphosphine / tetrahydrofuran
2: HCl / CH2Cl2; diethyl ether
View Scheme
参考文献
Kurosu, Michio; Dey, Sevendu Sekhar; Crick, Dean C.
Tetrahedron Letters, 2006 , vol. 47, # 28 p. 4871 - 4875
反应条件
1: DIAD; polymer-bound triphenylphosphine / tetrahydrofuran
2: HCl / CH2Cl2; diethyl ether
View Scheme
参考文献
Kurosu, Michio; Dey, Sevendu Sekhar; Crick, Dean C.
Tetrahedron Letters, 2006 , vol. 47, # 28 p. 4871 - 4875