3,6-二硝基-9H-咔唑合成路线 （共 16 条）
反应条件
hydrogen; palladium on activated charcoal in tetrahydrofuran 96 h;
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , # 9 p. 1727 - 1734
反应条件
Chlorieren in Eisessig;
参考文献
I.G.Farbenind.
Patent: DE761942 , 1941 ;
DRP/DRBP Org.Chem.
反应条件
1: 1.) K2CO3 / 1.) DMF, from 40 to 60 deg C, 1.5 h, 2.) DMF, a) RT, 2 h, b) from 45 to 55 deg C, 1 h 2: H2 / 10percent Pd/C / methanol; acetic acid / 5.5 h / 760 Torr View Scheme
参考文献
Galan, Amalia; De Mendoza, Javier; Toiron, Catherine; Bruix, Marta; Deslongchamps, Ghislain; Rebek Jr., Julius
Journal of the American Chemical Society, 1991 , vol. 113, # 24 p. 9424 - 9425
反应条件
1: sodium hydroxide / tetrahydrofuran / Reflux
2: palladium 10 on activated carbon; hydrazine / ethanol; water
View Scheme
参考文献
Chen, Zheng; Dreyer, Daniel R.; Wu, Zong-Quan; Wiggins, Kelly M.; Jiang, Zhenhua; Bielawski, Christopher W.
Journal of Polymer Science, Part A: Polymer Chemistry, 2011 , vol. 49, # 6 p. 1421 - 1426
反应条件
dichloro-acetic acid; bromine
参考文献
I.G.Farbenind.
Patent: DE761942 , 1941 ;
DRP/DRBP Org.Chem.
反应条件
dichloro-acetic acid; bromine
参考文献
I.G.Farbenind.
Patent: DE761942 , 1941 ;
DRP/DRBP Org.Chem.
