2-[(1E,3E,5E,7E)-9-甲氧基-3,7-二甲基壬-1,3,5,7-四烯基]-1,3,3-三甲基环己烯合成路线 （共 23 条）
反应条件
pyridine; trichlorophosphate in toluene T=50°C;
参考文献
Subramanian; Padmakumar; Bhat, Sujata V.
Tetrahedron Letters, 1997 , vol. 38, # 14 p. 2585 - 2586
反应条件
sodium ethanolate in ethanol Heating;
参考文献
Lee, Jun Sup; Jeong, Young Cheol; Ji, Minkoo; Baik, Woonphil; Lee, Sijoon; Koo, Sangho
Synlett, 2004 , # 11 p. 1937 - 1940
反应条件
n-butyllithium; Petroleum ether; benzene anschliessendes Behandeln mit Dimethylsulfat in Benzol bei 70grad in gedaempftem Licht;
参考文献
Hanze et al.
Journal of the American Chemical Society, 1946 , vol. 68, p. 1389
Journal of the American Chemical Society, 1948 , vol. 70, p. 1253,1255
反应条件
1.1: t-BuOK / dimethylformamide / -20 °C 1.2: 98 percent / dimethylformamide / -20 °C 2.1: 83 percent / NaOEt / ethanol / Heating View Scheme
参考文献
Lee, Jun Sup; Jeong, Young Cheol; Ji, Minkoo; Baik, Woonphil; Lee, Sijoon; Koo, Sangho
Synlett, 2004 , # 11 p. 1937 - 1940
反应条件
1.1: t-BuOK / dimethylformamide / -20 °C 1.2: 98 percent / dimethylformamide / -20 °C 2.1: 83 percent / NaOEt / ethanol / Heating View Scheme
参考文献
Lee, Jun Sup; Jeong, Young Cheol; Ji, Minkoo; Baik, Woonphil; Lee, Sijoon; Koo, Sangho
Synlett, 2004 , # 11 p. 1937 - 1940
反应条件
1.1: 80 percent / dimethylformamide 2.1: t-BuOK / dimethylformamide / -20 °C 2.2: 98 percent / dimethylformamide / -20 °C 3.1: 83 percent / NaOEt / ethanol / Heating View Scheme
参考文献
Lee, Jun Sup; Jeong, Young Cheol; Ji, Minkoo; Baik, Woonphil; Lee, Sijoon; Koo, Sangho
Synlett, 2004 , # 11 p. 1937 - 1940
反应条件
1: 73 percent / LiHMDS / tetrahydrofuran / -90 °C 2: 67 percent / pyridine / 1 h / Heating 3: 54 percent / POCl3, pyridine / toluene / 50 °C View Scheme
参考文献
Subramanian; Padmakumar; Bhat, Sujata V.
Tetrahedron Letters, 1997 , vol. 38, # 14 p. 2585 - 2586
反应条件
1: 73 percent / LiHMDS / tetrahydrofuran / -90 °C 2: 67 percent / pyridine / 1 h / Heating 3: 54 percent / POCl3, pyridine / toluene / 50 °C View Scheme
参考文献
Subramanian; Padmakumar; Bhat, Sujata V.
Tetrahedron Letters, 1997 , vol. 38, # 14 p. 2585 - 2586
反应条件
1: 67 percent / pyridine / 1 h / Heating 2: 54 percent / POCl3, pyridine / toluene / 50 °C View Scheme
参考文献
Subramanian; Padmakumar; Bhat, Sujata V.
Tetrahedron Letters, 1997 , vol. 38, # 14 p. 2585 - 2586
反应条件
potassium acetate; toluene
参考文献
Hoffmann-La Roche
Patent: US2451736 , 1946 ;
