反应条件
1: 75 percent / NBS 2: 74 percent / hexamethylenetetramine 3: tetrahydrofuran / Ambient temperature 4: BH3*Me2S / tetrahydrofuran 5: 1) Amberlyst, 2) NaBH4 / 2) MeOH, 50 deg C, 3) MeOH, RT 6: 90 percent / NaOH / methanol View Scheme
参考文献
Fang, Qun K.; Senanayake, Chris H.; Wilkinson, H. Scott; Waid, Stephen A.; Li, Hui
Tetrahedron Letters, 1998 , vol. 39, # 18 p. 2701 - 2704