3-(四氢呋喃-3-基)-3-氧代丙酸乙酯合成路线 (共 2 条)
反应条件
palladium 10 on activated carbon; hydrogen in tetrahydrofuran T=25°C; P=750.075 Torr; 24 h;
参考文献
Stefane, Bogdan; Polanc, Slovenko
Tetrahedron, 2009 , vol. 65, # 11 p. 2339 - 2343
反应条件
1: ethyl acetate With lithium hexamethyldisilazane in tetrahydrofuran; hexanes T=-78°C; 0.5 h; 2: methyl tetrahydrofuran-3-carboxylate in tetrahydrofuran; hexanes T=-78°C; 4 h;
参考文献
US2008/194577 A1, ;
Page/Page column 26 ;
US 20080194577 A1