(二苯基膦基)甲硫醇S-乙酸酯合成路线 （共 9 条）
反应条件
1,4-diaza-bicyclo[2.2.2]octane in toluene T=40°C; 4 h;
参考文献
WISCONSIN ALUMNI RESEARCH FOUNDATION
Patent: WO2003/104243 A1, 2003 ;
Location in patent: Page 20 ;
反应条件
trichlorosilane in chloroform 72 h;
参考文献
Nilsson, Bradley L.; Kiessling, Laura L.; Raines, Ronald T.
Organic Letters, 2001 , vol. 3, # 1 p. 9 - 12
反应条件
in toluene T=100°C; Inert atmosphere;
参考文献
Van Overschelde, Michel; Vervecken, Elias; Modha, Sachin G.; Cogen, Simon; Van der Eycken, Erik; Van der Eycken, Johan
Tetrahedron, 2009 , vol. 65, # 32 p. 6410 - 6415
反应条件
1: dimethylformamide 2: trichlorosilane / CHCl3 / 72 h View Scheme
参考文献
Nilsson, Bradley L.; Kiessling, Laura L.; Raines, Ronald T.
Organic Letters, 2001 , vol. 3, # 1 p. 9 - 12
反应条件
T=20°C; 1 h; Inert atmosphere;
参考文献
Sowa, Sylwia; Muehlberg, Michaela; Pietrusiewicz, K. Michal; Hackenberger, Christian P.R.
Bioorganic and Medicinal Chemistry, 2013 , vol. 21, # 12 p. 3465 - 3472
反应条件
sodium hydroxide in methanol
参考文献
WISCONSIN ALUMNI RESEARCH FOUNDATION
Patent: WO2003/104243 A1, 2003 ;
Location in patent: Page 21 ;
反应条件
N-ethyl-N,N-diisopropylamine in N,N-dimethyl-formamide T=20°C; Staudinger ligation; 12 h;
参考文献
Muehlberg, Michaela; Jaradat, Da'san M.M.; Kleineweischede, Rolf; Papp, Ilona; Dechtrirat, Decha; Muth, Silvia; Broncel, Malgorzata; Hackenberger, Christian P.R.
Bioorganic and Medicinal Chemistry, 2010 , vol. 18, # 11 p. 3679 - 3686
反应条件
1,4-diaza-bicyclo[2.2.2]octane in DMF-d7 T=25°C; Staudinger reaction; 12 h; Inert atmosphere;
参考文献
Kleineweischede, Rolf; Hackenberger, Christian P. R.
Angewandte Chemie - International Edition, 2008 , vol. 47, # 32 p. 5984 - 5988
反应条件
in tetrahydrofuran; water
T=20°C; 12 h;
参考文献
Nilsson, Bradley L.; Kiessling, Laura L.; Raines, Ronald T.
Organic Letters, 2001 , vol. 3, # 1 p. 9 - 12
