3-甲氧基苯硼酸频哪醇酯合成路线 (共 27 条)
反应条件
1.1: magnesium / tetrahydrofuran; toluene / 60 - 80 °C / |Inert atmosphere 1.2: 0 °C / |Inert atmosphere 1.3: 20 °C / |Inert atmosphere 2.1: toluene / 2.5 h / |Inert atmosphere; |Reflux View Scheme
参考文献
Tetrahedron Letters, , vol. 53, # 46 p. 6182 - 6185,4
反应条件
in diethyl ether T=20°C; 4 h;
参考文献
Advanced Synthesis and Catalysis, , vol. 355, # 6 p. 1083 - 1088
反应条件
iridium(hydrotris(pyrazolyl)borate)(1,5-cyclooctadiene) T=120°C; 16 h; Title compound not separated from byproducts.;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 79, # 12 p. 1980 - 1982
反应条件
polystyrene boronic acid; trifluoroacetic acid in acetonitrile 18 h; Heating;
参考文献
Tetrahedron Letters, , vol. 45, # 35 p. 6657 - 6660
反应条件
gold(III) chloride; N-bromosuccinmide in 1,2-dichloro-ethane T=20°C; 6 h; regioselective reaction;
参考文献
Qiu, Di; Mo, Fanyang; Zheng, Zhitong; Zhang, Yan; Wang, Jianbo
Organic Letters, 2010 , vol. 12, # 23 p. 5474 - 5477
反应条件
gold(III) chloride; N-iodo-succinimide in 1,2-dichloro-ethane T=20°C; 6 h; regioselective reaction;
参考文献
Qiu, Di; Mo, Fanyang; Zheng, Zhitong; Zhang, Yan; Wang, Jianbo
Organic Letters, 2010 , vol. 12, # 23 p. 5474 - 5477
反应条件
potassium tetrachloropalladate; cesium fluoride
T=70°C; Suzuki coupling; 3 h; Inert atmosphere;
参考文献
Bej, Ansuman; Srimani, Dipankar; Sarkar, Amitabha
Green Chemistry, 2012 , vol. 14, # 3 p. 661 - 667