3,5-二甲基苯硼酸频哪醇酯合成路线 (共 42 条)
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium hydroxide in tert-butyl methyl ether; water T=80°C; Suzuki-Miyaura coupling; 3 h;
参考文献
Harrisson, Peter; Morris, James; Steel, Patrick G.; Marder, Todd B.
Synlett, 2009 , # 1 p. 147 - 150
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium hydroxide in tert-butyl methyl ether; water T=80°C; Suzuki-Miyaura coupling; 3 h;
参考文献
Harrisson, Peter; Morris, James; Steel, Patrick G.; Marder, Todd B.
Synlett, 2009 , # 1 p. 147 - 150
反应条件
sodium hydroxide; hydroxylamine hydrochloride in ethanol T=20°C; 18 h;
参考文献
Tetrahedron Letters, , vol. 48, # 15 p. 2713 - 2715
反应条件
gold(III) chloride; N-iodo-succinimide in 1,2-dichloro-ethane T=40°C; 7 h; regioselective reaction;
参考文献
Qiu, Di; Mo, Fanyang; Zheng, Zhitong; Zhang, Yan; Wang, Jianbo
Organic Letters, 2010 , vol. 12, # 23 p. 5474 - 5477
反应条件
gold(III) chloride; N-bromosuccinmide in 1,2-dichloro-ethane T=40°C; 6 h; regioselective reaction;
参考文献
Qiu, Di; Mo, Fanyang; Zheng, Zhitong; Zhang, Yan; Wang, Jianbo
Organic Letters, 2010 , vol. 12, # 23 p. 5474 - 5477
反应条件
Cu(NO3)2*3H2O; cesium fluoride in methanol; water T=100°C; 5 h;
参考文献
Liskey, Carl W.; Liao, Xuebin; Hartwig, John F.
Journal of the American Chemical Society, 2010 , vol. 132, # 33 p. 11389 - 11391
反应条件
copper(l) iodide; 1,10-phenanthroline; potassium iodide in methanol; water T=80°C; 1 h; High pressure;
参考文献
Partridge, Benjamin M.; Hartwig, John F.
Organic Letters, 2013 , vol. 15, # 1 p. 140 - 143
反应条件
gold(III) chloride; N-chloro-succinimide in 1,2-dichloro-ethane
T=80°C; 48 h; regioselective reaction;
参考文献
Qiu, Di; Mo, Fanyang; Zheng, Zhitong; Zhang, Yan; Wang, Jianbo
Organic Letters, 2010 , vol. 12, # 23 p. 5474 - 5477
反应条件
bis-triphenylphosphine-palladium(II) chloride; potassium carbonate in ethanol; water; toluene
Suzuki-Miyaura Coupling; 14 h; Inert atmosphereReflux;
参考文献
Durak, Landon J.; Lewis, Jared C.
Organometallics, 2014 , vol. 33, # 3 p. 620 - 623
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium hydroxide in tert-butyl methyl ether; water
T=80°C; Suzuki-Miyaura coupling; 3 h;
参考文献
Harrisson, Peter; Morris, James; Steel, Patrick G.; Marder, Todd B.
Synlett, 2009 , # 1 p. 147 - 150