2,6-二甲基吡啶-4-硼酸频那醇酯合成路线 (共 6 条)
反应条件
1: 4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl-4',4',5',5'-tetramethyl-1,3,2-dioxaborolane With bis(η4-1,5-cyclooctadiene)-di-μ-methoxy-diiridium(I); 4,4'-di-tert-butyl-2,2'-dipyridyl in tert-butyl methyl ether Inert atmosphere; 2: 2,6-dimethylpyridine in tert-butyl methyl ether T=80°C; 0.0833333 h; Inert atmosphereMicrowave irradiation;
参考文献
Obligacion, Jennifer V.; Semproni, Scott P.; Chirik, Paul J.
Journal of the American Chemical Society, 2014 , vol. 136, # 11 p. 4133 - 4136
反应条件
(pentamethylcyclopentadienyl)Rh(.eta.4-hexamethylbenzene) T=150°C; 6 h;
参考文献
Cho; Iverson; Smith III
Journal of the American Chemical Society, 2000 , vol. 122, # 51 p. 12868 - 12869
反应条件
copper(ll) bromide in methanol T=80°C;
参考文献
Murphy, Jaclyn M.; Liao, Xuebin; Hartwig, John F.
Journal of the American Chemical Society, 2007 , vol. 129, # 50 p. 15434 - 15435
反应条件
Cu(NO3)2*3H2O; cesium fluoride in methanol; water T=100°C; 4 h;
参考文献
Liskey, Carl W.; Liao, Xuebin; Hartwig, John F.
Journal of the American Chemical Society, 2010 , vol. 132, # 33 p. 11389 - 11391
反应条件
copper dichloride in methanol T=90°C;
参考文献
Murphy, Jaclyn M.; Liao, Xuebin; Hartwig, John F.
Journal of the American Chemical Society, 2007 , vol. 129, # 50 p. 15434 - 15435
反应条件
copper(l) iodide; 1,10-phenanthroline; potassium iodide in methanol; water T=80°C; 1 h; High pressure;
参考文献
Partridge, Benjamin M.; Hartwig, John F.
Organic Letters, 2013 , vol. 15, # 1 p. 140 - 143