2,4-己二炔-1,6-二基 双(4-甲基苯磺酸酯)合成路线 （共 5 条）
反应条件
potassium hydroxide in tetrahydrofuran; water T=-15°C; 3 h;
参考文献
Rubin, Yves; Lin, Sophia S.; Knobler, Carolyn B.; Anthony, John; Boldi, Armen M.; Diederich, Francois
Journal of the American Chemical Society, 1991 , vol. 113, # 18 p. 6943 - 6949
反应条件
N,N,N',N,-tetramethylethylenediamine; 1-n-butyl-3-methylimidazolium hexafluorophosphate; copper(l) chloride T=20°C; Glaser oxidative coupling; 6.5 h;
参考文献
Yadav; Reddy; Reddy, K. Bhaskar; Gayathri, K. Uma; Prasad
Tetrahedron Letters, 2003 , vol. 44, # 34 p. 6493 - 6496
参考文献
Gao, Kunxiu; Goroff, Nancy S.
Journal of the American Chemical Society, 2000 , vol. 122, # 38 p. 9320 - 9321
反应条件
n-butyllithium in tetrahydrofuran; hexane T=-78 - -30°C;
参考文献
Rubin, Yves; Lin, Sophia S.; Knobler, Carolyn B.; Anthony, John; Boldi, Armen M.; Diederich, Francois
Journal of the American Chemical Society, 1991 , vol. 113, # 18 p. 6943 - 6949
反应条件
potassium carbonate in acetone 41 h; Ambient temperature;
参考文献
Hernandez; Galan; Rovira; Veciana
Synthesis, 1992 , # 11 p. 1164 - 1169
