mixt. of educts stirred for 2-3 h, molar ratio of Rb<BCl4> and N2O4 1:4 at -30 - -20°C in excess of NOCl; NOCl freezing in liq. N2;
参考文献
Titova, K. V.; Rosolovskii, V. Ya.
Russian Journal of Inorganic Chemistry (Translation of Zhurnal Neorganicheskoi Khimii), 1971 , vol. 16, p. 767 - 768
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Gmelin Handbook: B: B-Verb.8, 7.3, page 104 - 105
