16-氧杂双环[10.4.0]十六碳-17-烯合成路线 （共 12 条）
反应条件
toluene-4-sulfonic acid in toluene 3 h; Heating;
参考文献
Zakharkin, L. I.; Churilova, I. M.
Russian Chemical Bulletin, 1994 , vol. 43, # 4 p. 608 - 611
Izvestiya Akademi Nauk, Seriya Khimicheskaya, 1994 , # 4 p. 659 - 661
反应条件
1: 70 percent / KOH / 10 h / 80 - 90 °C 2: 80 percent / HClO4 / ethyl acetate / 12 h / 20 °C 3: p-TsOH / ethanol View Scheme
参考文献
Ogibin; Terent'ev; Nikishin
Russian Chemical Bulletin, 1998 , vol. 47, # 6 p. 1166 - 1169
反应条件
toluene-4-sulfonic acid Heating;
参考文献
Ogibin; Terent'ev; Nikishin
Russian Chemical Bulletin, 1998 , vol. 47, # 6 p. 1166 - 1169
反应条件
1: 86 percent / H2, HClO4 / Pd/C / ethyl acetate / 6 h / 20 °C 2: p-TsOH / Heating View Scheme
参考文献
Zakharkin, L. I.; Churilova, I. M.
Russian Chemical Bulletin, 1994 , vol. 43, # 4 p. 608 - 611
Izvestiya Akademi Nauk, Seriya Khimicheskaya, 1994 , # 4 p. 659 - 661
反应条件
trifluoromethylsulfonic anhydride; N-ethyl-N,N-diisopropylamine in toluene 1.) -78 deg C, 5 h, 2.) from -78 deg C to 0 deg C, 3.) 12 h, RT; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Hanaki, Naoyuki; Ishihara, Kazuaki; Kaino, Makoto; Naruse, Yuji; Yamamoto, Hisashi
Tetrahedron, 1996 , vol. 52, # 21 p. 7297 - 7320
反应条件
toluene-4-sulfonic acid in ethanol
参考文献
Zakharkin, L. I.; Churilova, I. M.
Russian Chemical Bulletin, 1994 , vol. 43, # 4 p. 608 - 611
Izvestiya Akademi Nauk, Seriya Khimicheskaya, 1994 , # 4 p. 659 - 661
反应条件
2: 72 percent / dibenzo-18-crown-6 / dioxane / 7 h / Heating 3: p-TsOH / ethanol View Scheme
参考文献
Zakharkin, L. I.; Churilova, I. M.
Russian Chemical Bulletin, 1994 , vol. 43, # 4 p. 608 - 611
Izvestiya Akademi Nauk, Seriya Khimicheskaya, 1994 , # 4 p. 659 - 661
反应条件
1: 72 percent / dibenzo-18-crown-6 / dioxane / 7 h / Heating 2: p-TsOH / ethanol View Scheme
参考文献
Zakharkin, L. I.; Churilova, I. M.
Russian Chemical Bulletin, 1994 , vol. 43, # 4 p. 608 - 611
Izvestiya Akademi Nauk, Seriya Khimicheskaya, 1994 , # 4 p. 659 - 661
反应条件
1: 70 percent / ethanol; dioxane / 22 h / Heating View Scheme
参考文献
Mahajan, Jaswant Rai; Araujo, Hugo Clemente
Synthesis, 1980 , # 1 p. 64 - 66
反应条件
Yield given. Multistep reaction;
参考文献
Mahajan, Jaswant Rai; Araujo, Hugo Clemente
Synthesis, 1980 , # 1 p. 64 - 66
