4-氧代-3,4-二氢吡啶-1(2H)-羧酸叔丁酯合成路线 （共 3 条）
反应条件
K(iPrO)3BH in tetrahydrofuran; diethyl ether; isopropyl alcohol T=-15°C; 1 h;
参考文献
Pizzuti, Maria Gabriella; Minnaard, Adriaan J.; Feringa, Ben L.
Organic and Biomolecular Chemistry, 2008 , vol. 6, # 19 p. 3464 - 3466
反应条件
1: 4-methoxy pyridine With K(iPrO)3BH in tetrahydrofuran T=-41°C; 0.25 h; 2: phenyl chloroformate in tetrahydrofuran T=-41°C; 2 h; 3: potassium tert-butylate in tetrahydrofuran T=-41 - 20°C; 2.5 h;
参考文献
EP1204659 B1, ;
Page/Page column 31 ;
反应条件
palladium (II) trifluoroacetate; oxygen; dimethyl sulfoxide T=80°C; P=760.051 Torr; 48 h;
参考文献
Diao, Tianning; Stahl, Shannon S.
Journal of the American Chemical Society, 2011 , vol. 133, # 37 p. 14566 - 14569
