(R)-(+)-1-辛炔-3-醇合成路线 (共 41 条)
反应条件
NB-Enantrane 48 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 47, # 14 p. 2814 - 2816
反应条件
tetrabutyl ammonium fluoride Yield given;
参考文献
Tetrahedron Letters, , vol. 30, # 50 p. 7083 - 7086
反应条件
recombinant N-terminally strep-tag Pseudomonas aeruginosa arylsulfatase; water in aq. buffer pH=8; 6 h; Enzymatic reaction; enantioselective reaction;
参考文献
Angewandte Chemie - International Edition, , vol. 52, # 11 p. 3277 - 3279
Angew. Chem., , vol. 125, # 11 p. 3359 - 3361,3
反应条件
lithium amide in tetrahydrofuran; ammonia T=-78°C; other base and conditions; Product distribution;
参考文献
Tetrahedron Letters, , vol. 30, # 50 p. 7083 - 7086
反应条件
9-borabicyclo[3.3.1]nonane dimer; (+)-(R)-α-pinene; acetaldehyde 0 degC then allowing to warm to room temperature; Title compound not separated from byproducts;
参考文献
Tetrahedron, , vol. 40, # 8 p. 1371 - 1380
反应条件
in acetone Ambient temperaturephosphate buffer, pH 7, Lipase PPL; Yield given. Yields of byproduct given;
参考文献
Chemistry Letters, , # 1 p. 107 - 110
反应条件
n-butyllithium; triphenylphosphine 1.) CCl4, 4 h, reflux; 2.) THF, -35 deg C; Yield given. Multistep reaction;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 18 p. 1344 - 1345
反应条件
in acetone Ambient temperaturephosphate buffer, pH 7, Lipase PPL; Yield given. Yields of byproduct given;
参考文献
Chemistry Letters, , # 1 p. 107 - 110
反应条件
phosphate buffer; Pseudomonas lipase Amano AH; (2R-trans)-2-(3,4-dihydroxyphenyl)-3,4-dihydro-2H-1-benzopyran-3,5,7-triol T=30°C; pH=7.0; 144 h; Product distribution; Further Variations:Reagents;
参考文献
Tetrahedron Asymmetry, , vol. 13, # 4 p. 415 - 422
反应条件
T=28°C; 48 h; culture broth of Bacillus subtilis var. Niger; further microorganisms or their esterase; other reaction conditions; Product distribution;
参考文献
Agricultural and Biological Chemistry, , vol. 44, # 10 p. 2407 - 2412