(S)-1-辛炔-3-醇合成路线 （共 46 条）
反应条件
(-)-(S)-BINAL-H in tetrahydrofuran 1.) -100 deg C, 1 h; 2.) -78 deg C, 2 h; Title compound not separated from byproducts;
参考文献
Noyori, R.; Tomino, I.; Yamada, M.; Nishizawa, M.
Journal of the American Chemical Society, 1984 , vol. 106, # 22 p. 6717 - 6725
反应条件
potassium carbonate in methanol 16 h;
参考文献
Abad, Jose-Luis; Villorbina, Gemma; Fabrias, Gemma; Camps, Francisco
Journal of Organic Chemistry, 2004 , vol. 69, # 21 p. 7108 - 7113
反应条件
sodium hydride in tetrahydrofuran T=0°C; 1 h;
参考文献
Tetrahedron Letters, , vol. 34, # 41 p. 6587 - 6590
反应条件
potassium hydroxide in ethanol T=40°C; 1.5 h;
参考文献
Hashimoto; Kase; Suzuki; Yanagiya; Ikegami
Synthetic Communications, 1991 , vol. 21, # 6 p. 833 - 839
参考文献
Tetrahedron: Asymmetry, , vol. 4, # 7 p. 1645 - 1650
Tetrahedron Asymmetry, , vol. 8, # 21 p. 3597 - 3601
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran Ambient temperature;
参考文献
Shimizu, Makoto; Kawanami, Hiroshi; Fujisawa, Tamotsu
Chemistry Letters, 1992 , # 1 p. 107 - 110
反应条件
sodium sulfate; Birman's catalyst in chloroform T=0°C; 6 h;
参考文献
Organic Letters, , vol. 8, # 21 p. 4859 - 4861
反应条件
NB-Enantrane 48 h; Ambient temperatureother α,β-acetylenic ketones; Product distribution;
参考文献
Midland, Mark M.; Kazubski, Aleksander
Journal of Organic Chemistry, 1982 , vol. 47, # 14 p. 2814 - 2816
反应条件
lithium amide; ammonia
参考文献
Yadav; Deshpande; Sharma
Tetrahedron, 1992 , vol. 48, # 21 p. 4465 - 4474
反应条件
1: 91 percent / TiCl4 / CH2Cl2 / -78 °C 2: 97 percent / PCC 3: aq. KOH / methanol View Scheme
参考文献
Journal of the American Chemical Society, , vol. 105, # 9 p. 2904 - 2905
