(S)-1-辛炔-3-醇合成路线 （共 46 条）
反应条件
1: 97 percent / PCC 2: aq. KOH / methanol View Scheme
参考文献
Journal of the American Chemical Society, , vol. 105, # 9 p. 2904 - 2905
反应条件
potassium hydroxide in methanol Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of the American Chemical Society, , vol. 105, # 9 p. 2904 - 2905
参考文献
Chandrasekharam; Liu
Journal of Organic Chemistry, 1998 , vol. 63, # 24 p. 9122 - 9124
反应条件
1: pyridine / 12 h / 0 °C 2: 95 percent / hydrogen / Rh (5 percent on alumina) / ethyl acetate / 20 °C 3: K2CO3; Na2SO4; MeOH 4: CCl4; Ph3P; NaHCO3 / Heating 5: LDA / tetrahydrofuran / -70 - 20 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 41, # 6 p. 823 - 826
反应条件
1: 95 percent / hydrogen / Rh (5 percent on alumina) / ethyl acetate / 20 °C 2: K2CO3; Na2SO4; MeOH 3: CCl4; Ph3P; NaHCO3 / Heating 4: LDA / tetrahydrofuran / -70 - 20 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 41, # 6 p. 823 - 826
反应条件
n-butyllithium in tetrahydrofuran
参考文献
Tetrahedron Letters, , vol. 31, # 31 p. 4495 - 4496
反应条件
CAL-B in di-isopropyl ether T=30°C; Esterification; 10 h; Enzymatic reaction; Title compound not separated from byproducts.;
参考文献
Journal of Organic Chemistry, , vol. 65, # 1 p. 83 - 88
反应条件
immobilized Candida antarctica Lipase B in di-isopropyl ether T=25°C; Enzymatic reaction;
参考文献
Abad, Jose-Luis; Villorbina, Gemma; Fabrias, Gemma; Camps, Francisco
Journal of Organic Chemistry, 2004 , vol. 69, # 21 p. 7108 - 7113
反应条件
Candida antarctica lipase in di-isopropyl ether T=25°C; 2 h; Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 68, # 13 p. 5351 - 5356
反应条件
1: (S)-(+)-(1-methylpyrrolidin-2-yl)diphenylmethanol / toluene / -20 °C 2: 90 percent / NaOH / methanol / 3 h / Ambient temperature View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 4 p. 937 - 943
