2-溴-5-(三甲基硅基)吡啶合成路线 (共 2 条)
反应条件
1: 2,5-dibromo-pyridine With n-butyllithium in diethyl ether; hexane T=-90°C; 1 h; 2: chloro-trimethyl-silane in diethyl ether; hexane T=-90°C; 1 h;
参考文献
Stange, Andreas F.; Tokura, Satoshi; Kira, Mitsuo
Journal of Organometallic Chemistry, 2000 , vol. 612, # 1-2 p. 117 - 124
反应条件
n-butyllithium in toluene T=-78 - 25°C; Alkylation;
参考文献
Wang, Xin; Rabbat, Philippe; O'Shea, Paul; Tillyer, Richard; Grabowski; Reider, Paul J.
Tetrahedron Letters, 2000 , vol. 41, # 22 p. 4335 - 4338