1: With N,N-dimethyl-formamide; trichlorophosphate T=0 - 70°C; 4 h; 2: With sodium hydroxide in water T=60°C; 0.0833333 h; Cooling;
参考文献
PRESIDENT AND FELLOWS OF HARVARD COLLEGE; SHANGHAI INSTITUTE OF ORGANIC CHEMISTRY, CHINESE ACADEMY OF SCIENCES; YUAN, Junying; YUAN, Chengye; DEGTEREV, Alexei
Patent: WO2010/75290 A1, 2010 ;
Location in patent: Page/Page column 44-45 ;
