甲基 1,3-苯并二恶唑-5-羧酸酯合成路线 （共 49 条）
反应条件
1: 86 percent / I2; AgO2CCF3 / methanol; CHCl3 / 16 h / 18 °C 2: 93 percent / pyridinium chlorochromate / CH2Cl2 / 16 h / 18 °C 3: 88 percent / acetic acid; sodium cyanide; MnO2 / CHCl3 / 16 h / 18 °C 4: 24 percent / triethylamine / PdCl2(dppf) / acetonitrile / 0.25 h / 80 °C / microwave irradiation View Scheme
参考文献
Organic Letters, , vol. 9, # 18 p. 3683 - 3685
反应条件
1: 88 percent / acetic acid; sodium cyanide; MnO2 / CHCl3 / 16 h / 18 °C 2: 24 percent / triethylamine / PdCl2(dppf) / acetonitrile / 0.25 h / 80 °C / microwave irradiation View Scheme
参考文献
Organic Letters, , vol. 9, # 18 p. 3683 - 3685
反应条件
dihydrogen peroxide; sulfuric acid in methanol 24 h; Ambient temperature;
参考文献
Journal of Organic Chemistry, , vol. 49, # 24 p. 4740 - 4741
反应条件
water in acetonitrile T=25°C; Kinetics;
参考文献
Bulletin of the Korean Chemical Society, , vol. 34, # 9 p. 2697 - 2701
反应条件
in methanol; benzene 0.5 h; Ambient temperature; Yield given;
参考文献
Chemical & Pharmaceutical Bulletin, , vol. 29, # 5 p. 1475 - 1478
反应条件
triethylamine in dichloromethane T=0 - 5°C; 2 h;
参考文献
Yang, Jinliang; Xu, Fei; Shi, Suqing; Nie, Jun
Photochemical and Photobiological Sciences, 2012 , vol. 11, # 8 p. 1377 - 1382
反应条件
oxygen; potassium carbonate T=60°C; P=750.075 Torr; 24 h; Schlenk techniqueGreen chemistry;
参考文献
Jagadeesh, Rajenahally V.; Junge, Henrik; Pohl, Marga-Martina; Radnik, Joerg; Brueckner, Angelika; Beller, Matthias
Journal of the American Chemical Society, 2013 , vol. 135, # 29 p. 10776 - 10782
反应条件
1: KOH / butan-1-ol 2: O2-O3; Zn; AcOH / methanol 3: 90 percent / I2; KOH View Scheme
参考文献
Journal of Pharmacology and Experimental Therapeutics, , vol. 299, # 2 p. 558 - 566
反应条件
1: O2-O3; Zn; AcOH / methanol 2: 90 percent / I2; KOH View Scheme
参考文献
Journal of Pharmacology and Experimental Therapeutics, , vol. 299, # 2 p. 558 - 566
反应条件
1: 73 percent / p-toluenesulfonic acid monohydrate; trimethyl orthoformate / 12 h / 20 °C 2: 78 percent / EtAlCl2 / CH2Cl2 / 1 h / -78 - 20 °C View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 71, # 9 p. 2181 - 2185
