苯并[1,3]二氧代l-5-乙酸甲酯合成路线 （共 26 条）
反应条件
in ClCH2 CH2 Cl; water
参考文献
CoCensys, Inc.
Patent: US5891871 A1, 1999 ;
US 5891871 A
反应条件
1: 39 percent / stannic chloride / CH2Cl2 / 22 h 2: 4.5 g / NaOH / ethanol / 14 h / Ambient temperature View Scheme
参考文献
Jones, David W.; Thompson, Adrian M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 21 p. 2533 - 2540
反应条件
perchloric acid in various solvent(s)
48 h; Ambient temperature;
参考文献
Costa, P. R. R.; Lopes, C. C.; Pinto, A. V.
Synthetic Communications, 1983 , vol. 13, # 8 p. 691 - 700
反应条件
tin(IV) chloride in 1,2-dichloro-ethane
1.5 h; Ambient temperature;
参考文献
Rizzacasa, Mark A.; Sargent, Melvyn V.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 2017 - 2022
反应条件
1: 78 percent / HClO4 / various solvent(s) / 48 h / Ambient temperature
2: 1.) CH3ONa, 2.) O2 / 1.) methanol, reflux
View Scheme
参考文献
Costa, P. R. R.; Lopes, C. C.; Pinto, A. V.
Synthetic Communications, 1983 , vol. 13, # 8 p. 691 - 700
反应条件
1: 72 percent / HClO4 / various solvent(s) / 48 h / Ambient temperature
2: 1.) CH3ONa, 2.) O2 / 1.) methanol, reflux
View Scheme
参考文献
Rizzacasa, Mark A.; Sargent, Melvyn V.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 2017 - 2022
