7-氯苯并[b]噻吩-3(2H)-酮合成路线 （共 6 条）
反应条件
sodium hydroxide in water 1 h; Heating;
参考文献
Rahman, Loay K. A.; Scrowston, Richard M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 3 p. 385 - 390
反应条件
1: 1.) NaNO3, hydrochloric acid, 2.) Na2S2, NaOH / 2.) H2O, room temperature, 2 h 2: 90 percent / Na2S2O4, Na2CO3 / H2O / 0.5 h / Heating 3: 70 percent / 1 h 4: 82 percent / anhyd. NaOAc / 1 h / Heating 5: 68 percent / 10percent NaOH / H2O / 1 h / Heating View Scheme
参考文献
Rahman, Loay K. A.; Scrowston, Richard M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 3 p. 385 - 390
反应条件
1: 70 percent / 1 h 2: 82 percent / anhyd. NaOAc / 1 h / Heating 3: 68 percent / 10percent NaOH / H2O / 1 h / Heating View Scheme
参考文献
Rahman, Loay K. A.; Scrowston, Richard M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 3 p. 385 - 390
反应条件
1: 90 percent / Na2S2O4, Na2CO3 / H2O / 0.5 h / Heating 2: 70 percent / 1 h 3: 82 percent / anhyd. NaOAc / 1 h / Heating 4: 68 percent / 10percent NaOH / H2O / 1 h / Heating View Scheme
参考文献
Rahman, Loay K. A.; Scrowston, Richard M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 3 p. 385 - 390
反应条件
1: 82 percent / anhyd. NaOAc / 1 h / Heating 2: 68 percent / 10percent NaOH / H2O / 1 h / Heating View Scheme
参考文献
Rahman, Loay K. A.; Scrowston, Richard M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 3 p. 385 - 390
反应条件
1: 90 percent / NaBH4 / ethanol / 1 h / Heating 2: 88 percent / conc. HCl / aq. ethanol / 3 h / Heating View Scheme
参考文献
Rahman, Loay K. A.; Scrowston, Richard M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 3 p. 385 - 390
