1: 69 percent / PCl5 / CH2Cl2 / 6 h / Heating 2: 600 °C / 0.01 Torr 3: 1000 °C / 0.01 Torr View Scheme
参考文献
Sarobe, Martin; Zwikker, Jan W.; Snoeijer, Judith D.; Wiersum, Ulfert E.; Jenneskens, Leonardus W.
Journal of the Chemical Society, Chemical Communications, 1994 , # 1 p. 89 - 90
phosphorus pentachloride in dichloromethane 6 h; Heating;
参考文献
Sarobe, Martin; Zwikker, Jan W.; Snoeijer, Judith D.; Wiersum, Ulfert E.; Jenneskens, Leonardus W.
Journal of the Chemical Society, Chemical Communications, 1994 , # 1 p. 89 - 90
1: N,N-dimethyl-formamide With trichlorophosphate T=10°C; Addition; 2: 1-Acetylpyrene in N,N-dimethyl-formamide Substitution; Vilsmeier reaction; 20 h; Title compound not separated from byproducts;
参考文献
Malakhov; Malakhova; Kuznitsova; Grechishnikova; Prokhorenko; Skorobogatyi; Korshun; Berlin
Russian Journal of Bioorganic Chemistry, 2000 , vol. 26, # 1 p. 34 - 44