(S)-(-)-2-溴丙酸合成路线 （共 23 条）
反应条件
bromine; isopentyl nitrite in dichloromethane Product distribution / selectivity;
参考文献
UNIVERSITY OF VIRGINIA PATENT FOUNDATION
Patent: WO2007/117404 A2, 2007 ;
Location in patent: Page/Page column 24-27 ;
反应条件
lithium hydroxide in tetrahydrofuran T=20°C; Hydrolysis; 0.0833333 h;
参考文献
Boyes, Scott A.; Hewson, Alan T.
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 16 p. 2759 - 2765
反应条件
iron oxide-Candida rugosa (E.C.3.1.1.3) lipase in hexane T=30°C; 168 h;
参考文献
Chemical Communications, , # 35 p. 4432 - 4434
反应条件
1: With n-butyllithium; diethylzinc; (S)-(+)-3-hydroxy-tetrahydrofuran in hexane; toluene T=-78 - 0°C; 13 h; 2: With hydrogenchloride in tetrahydrofuran T=20°C; 48 h; Title compound not separated from byproducts;
参考文献
Tetrahedron Letters, , vol. 42, # 34 p. 5985 - 5987
参考文献
Chemische Berichte, , vol. 33, p. 3355
Justus Liebigs Annalen der Chemie, , vol. 349, p. 325
Justus Liebigs Annalen der Chemie, , vol. 370, p. 236,237
Justus Liebigs Annalen der Chemie, , vol. 340, p. 171
Bulletin des Societes Chimiques Belges, , vol. 46, p. 485
反应条件
lithium hydroxide; dihydrogen peroxide in tetrahydrofuran 0.5 h; Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Tetrahedron: Asymmetry, , vol. 6, # 8 p. 1919 - 1932
参考文献
Chemische Berichte, , vol. 40, p. 491
Chemische Berichte, , vol. 39, p. 3988
Chem. Zentralbl., , vol. 77, # II p. 60
Justus Liebigs Annalen der Chemie, , vol. 340, p. 171
Chemische Berichte, , vol. 49, p. 2456
参考文献
Justus Liebigs Annalen der Chemie, , vol. 370, p. 236,237
Justus Liebigs Annalen der Chemie, , vol. 340, p. 171
Justus Liebigs Annalen der Chemie, , vol. 349, p. 325
Chemische Berichte, , vol. 33, p. 3354
参考文献
Justus Liebigs Annalen der Chemie, , vol. 340, p. 171
反应条件
barium dihydroxide T=37°C;
参考文献
Akasi
Journal of Biochemistry (Tokyo, Japan), 1937 , vol. 25, p. 283
Chem. Zentralbl., 1938 , vol. 109, # I p. 1133
Full Text Show Details
Herbst; Swart
Journal of Organic Chemistry, 1946 , vol. 11, p. 375
