Marchal, Joel; Bodiguel, Jacques; Fort, Yves; Caubere, Paul
Journal of Organic Chemistry, 1995 , vol. 60, # 26 p. 8336 - 8340
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反应条件
1: 5-bromo-5-(tributylstannyl)pentanal With 2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in benzene T=80°C; 4 h; 2: benzoyl chloride With triethylamine in benzene Further stages.;
copper(II) bis(trifluoromethanesulfonate); trilt;lt;2-(4R)-(4-phenyl-1,3-oxazolinyl)gt;methylgt;amine in acetone 40 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
