sulfuric acid; lithium bromide; [PdBr2(PPh3)2] in various solvent(s) T=120°C; P=45003.6 Torr; 12 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Beller, Matthias; Eckert, Markus; Geissler, Holger; Napierski, Bernd; Rebenstock, Heinz-Peter; Holla, E. Wolfgang
Chemistry - A European Journal, 1998 , vol. 4, # 5 p. 935 - 941
1: 3-methylsulfanyl-propionaldehyde; 3-(methylseleno)-propionaldehyde With sodium hydrogensulfite in water T=20°C; 0.166667 h; 2: sodium cyanide in water T=20°C; 2 h;
1: With pyrrolidine in methanol
T=20°C; 0.5 h; Inert atmosphere;
2: With sodium periodate
Inert atmosphere;
3: With 1,8-diazabicyclo[5.4.0]undec-7-ene in dichloromethane
Inert atmosphere;
参考文献
Erden, Ihsan; Sabol, Jenny; Gubeladze, Ana; Ruiz, Andrea
Turkish Journal of Chemistry, 2013 , vol. 37, # 4 p. 519 - 524
