2-苯基咪唑-5-羧酸乙酯合成路线 (共 10 条)
反应条件
thionyl chloride T=75°C; 17 h; Inert atmosphere;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 24, # 1 p. 262 - 267
反应条件
p-methoxyphenyl mercaptan 1 h; Inert atmosphereUV-irradiation;
参考文献
Smith, Matthew R.; Blake, Alexander J.; Hayes, Christopher J.; Stevens, Malcolm F. G.; Moody, Christopher J.
Journal of Organic Chemistry, 2009 , vol. 74, # 24 p. 9372 - 9380
反应条件
dodecacarbonyltriiron in 1,2-dichloro-ethane 1.) r.t., 4 h; 2.) 80 deg C, 20 h; Yields of byproduct given;
参考文献
Nakanishi, Saburo; Nantaku, Junji; Otsuji, Yoshio
Chemistry Letters, 1983 , p. 341 - 342
反应条件
1.1: sodium acetate / water / 0.5 h / 100 °C / |Inert atmosphere 1.2: |Inert atmosphere 2.1: sodium hydroxide / water / 22 h / 100 °C 3.1: thionyl chloride / 17 h / 75 °C / |Inert atmosphere View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 24, # 1 p. 262 - 267
反应条件
1: sodium hydroxide / water / 22 h / 100 °C 2: thionyl chloride / 17 h / 75 °C / |Inert atmosphere View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 24, # 1 p. 262 - 267
反应条件
1 h; Inert atmosphereUV-irradiation;
参考文献
Journal of Organic Chemistry, , vol. 74, # 24 p. 9372 - 9380
反应条件
sodium amalgam; water und Erwaermen des Reaktionsprodukts mit Benzimidsaeure-methylester in Aethanol;
参考文献
Journal of the Chemical Society, , p. 4225,4227
参考文献
Journal of the Chemical Society, , vol. 115, p. 1019
反应条件
1: diluted hydrochloric acid / 145 - 150 °C 2: alcoholic hydrochloric acid View Scheme
参考文献
Journal of the Chemical Society, , vol. 115, p. 1019
反应条件
2: diluted hydrochloric acid / 145 - 150 °C 3: alcoholic hydrochloric acid View Scheme
参考文献
Journal of the Chemical Society, , vol. 115, p. 1019