4-氯-3-三氟甲基异氰酸苯酯合成路线 (共 22 条)
反应条件
in dichloromethane
T=0 - 20°C; Inert atmosphere;
参考文献
Wang, Ke; Li, Yan; Zhang, Li-Jing; Chen, Xiao-Guang; Feng, Zhi-Qiang
Chinese Chemical Letters, 2014 , vol. 25, # 5 p. 702 - 704
反应条件
1: dichloromethane / 16 h / 20 °C
2: trifluoroacetic acid; triethylsilane / dichloromethane / 16 h / 50 °C
3: sulfuric acid / water / 3 h / |Reflux
View Scheme
参考文献
SUZHOU ZELGEN BIOPHARMACEUTICAL CO., LTD.; Feng, Weidong; Gao, Xiaoyong; Dai, Xiaojun
Patent: US2013/35492 A1, 2013 ;