1.1: hydrogenchloride; sodium nitrite / water / 0.17 h / 0 - 5 °C
1.2: 1 h / 20 °C
2.1: 2-methyl-2-iodopropane / dichloromethane / 18 h / 20 °C / |Inert atmosphere
View Scheme
Clive, D. L. J.; Farina, Vittorio; Singh, Alok; Wong, Chi Kwong; Kiel, William, A.; Menchen, Steven M.
Journal of Organic Chemistry, 1980 , vol. 45, # 11 p. 2120 - 2126