2-(6-溴萘-2-基)乙酸合成路线 （共 7 条）
反应条件
sulfuric acid; acetic acid in water T=110°C; 24 h;
参考文献
Zhao, Wenjun; Huang, Li; Guan, Yong; Wulff, William D.
Angewandte Chemie - International Edition, 2014 , vol. 53, # 13 p. 3436 - 3441
Angew. Chem., 2014 , vol. 126, # 13 p. 3504 - 3509,6
反应条件
1: 95 percent / LAH / tetrahydrofuran / -10 °C 2: 99 percent / SOCl2; ZnCl2 / dioxane / -10 °C 3: 97 percent / H2O; acetonitrile / Heating 4: 93 percent / aq. AcOH / H2SO4 / Heating View Scheme
参考文献
Pu, Yu-Ming; Ku, Yi-Yin; Grieme, Timothy; Black, Lawrence A.; Bhatia, Ashok V.; Cowart, Marion
Organic Process Research and Development, 2007 , vol. 11, # 6 p. 1004 - 1009
反应条件
1: 99 percent / SOCl2; ZnCl2 / dioxane / -10 °C 2: 97 percent / H2O; acetonitrile / Heating 3: 93 percent / aq. AcOH / H2SO4 / Heating View Scheme
参考文献
Pu, Yu-Ming; Ku, Yi-Yin; Grieme, Timothy; Black, Lawrence A.; Bhatia, Ashok V.; Cowart, Marion
Organic Process Research and Development, 2007 , vol. 11, # 6 p. 1004 - 1009
反应条件
1: 97 percent / H2O; acetonitrile / Heating 2: 93 percent / aq. AcOH / H2SO4 / Heating View Scheme
参考文献
Pu, Yu-Ming; Ku, Yi-Yin; Grieme, Timothy; Black, Lawrence A.; Bhatia, Ashok V.; Cowart, Marion
Organic Process Research and Development, 2007 , vol. 11, # 6 p. 1004 - 1009
反应条件
1: bromine / 210 °C / Irradiation 2: aqueous ethanol / Erhitzen des Reaktionsprodukts mit wss.-aethanol. Kalilauge View Scheme
参考文献
Jones et al.
Journal of the American Chemical Society, 1948 , vol. 70, p. 2843,2945
反应条件
ethanol Erhitzen des Reaktionsprodukts mit wss.-aethanol. Kalilauge;
参考文献
Jones et al.
Journal of the American Chemical Society, 1948 , vol. 70, p. 2843,2945
反应条件
borane-THF in tetrahydrofuran
T=-15°C;
参考文献
Altenbach, Robert J.; Black, Lawrence A.; Chang, Sou-Jen; Cowart, Marlon D.; Faghih, Ramin; Gfesser, Gregory A.; Ku, Yi-yin; Liu, Huaqing; Lukin, Kirill A.; Nersesian, Diana L.; Pu, Yu-ming; Sharma, Padam N.; Bennani, Youssef L.
Patent: US2004/92521 A1, 2004 ;
Location in patent: Page/Page column 30-31 ;
US 20040092521 A1
