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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
1-碘-2-甲氧基萘
合成路线
（共 24 条）
32721-21-4
1-碘-2-甲氧基萘
+
135-19-3
2-萘酚
→
反应条件
93-04-9
2-萘甲醚
+
35193-70-5
(R)-2’-甲氧基-[1,1’]联萘-2-醇
反应条件
1: β-naphthol With potassium tert-butylate in dimethyl sulfoxide T=25°C; 0.25 h; Inert atmosphere; 2: 1-iodo-2-methoxy naphthalene in dimethyl sulfoxide T=25°C; 2 h; Inert atmosphereIrradiation; Kinetics;
参考文献
Tempesti, Tomas C.; Pierini, Adriana B.; Baumgartner, Maria T.
New Journal of Chemistry, 2009 , vol. 33, # 7 p. 1523 - 1528
32721-21-4
1-碘-2-甲氧基萘
→
反应条件
93-04-9
2-萘甲醚
反应条件
caesium carbonate; hydroquinone; palladium diacetate in N,N-dimethyl acetamide T=125°C; 48 h;
参考文献
Hennings, D. David; Iwama, Tetsuo; Rawal, Viresh H.
Organic Letters, 1999 , vol. 1, # 8 p. 1205 - 1208
32721-21-4
1-碘-2-甲氧基萘
→
反应条件
93-04-9
2-萘甲醚
+
75685-01-7
(S)-(-)-2,2’-二甲氧基-1,1’-联萘
反应条件
tetraethylammonium p-toluenesulfonate; bis-triphenylphosphine-palladium(II) chloride in N,N-dimethyl-formamide Ambient temperatureelectrolysis;
参考文献
Tetrahedron Letters, , vol. 26, # 13 p. 1655 - 1658
124-38-9
二氧化碳
+
32721-21-4
1-碘-2-甲氧基萘
→
反应条件
93-04-9
2-萘甲醚
+
947-62-6
2-甲氧基-1-萘甲酸
反应条件
tetraethylammonium p-toluenesulfonate; triphenylphosphine; bis-triphenylphosphine-palladium(II) chloride in N,N-dimethyl-formamide Pt anode/Pt cathode; electrolysis with 2.5 mA/cm2;
参考文献
Chemistry Letters, , p. 169 - 172
32721-21-4
1-碘-2-甲氧基萘
→
反应条件
93-04-9
2-萘甲醚
+
67886-69-5
2-碘-6-甲氧基萘
+
97825-82-6
反应条件
iodine; iodic acid in N,N-dimethyl-formamide T=80°C; 18 h; Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 50, # 19 p. 3649 - 3651
7498-57-9
2-萘乙腈
+
32721-21-4
1-碘-2-甲氧基萘
→
反应条件
93-04-9
2-萘甲醚
+
1363650-08-1
反应条件
1: 2-(2-naphthyl)acetonitrile With potassium tert-butylate in dimethyl sulfoxide 0.25 h; Inert atmosphere; 2: 1-iodo-2-methoxy naphthalene in dimethyl sulfoxide 3 h; Inert atmosphereIrradiation; regioselective reaction;
参考文献
New Journal of Chemistry, , vol. 36, # 3 p. 597 - 602
32721-21-4
1-碘-2-甲氧基萘
+
135-19-3
2-萘酚
→
反应条件
93-04-9
2-萘甲醚
+
35193-70-5
(R)-2’-甲氧基-[1,1’]联萘-2-醇
反应条件
1: β-naphthol With potassium tert-butylate in dimethyl sulfoxide T=25°C; 0.25 h; Inert atmosphere; 2: 1-iodo-2-methoxy naphthalene in dimethyl sulfoxide T=25°C; 2 h; Inert atmosphereIrradiation; Kinetics;
参考文献
New Journal of Chemistry, , vol. 33, # 7 p. 1523 - 1528
32721-21-4
1-碘-2-甲氧基萘
→
反应条件
74877-61-5
反应条件
1.1: lithium diisopropyl amide / tetrahydrofuran / -78 °C 1.2: 9 h / -78 - 20 °C 1.3: 50 °C / Inert atmosphere 2.1: water; potassium hydroxide / methanol / 12 h / 25 °C View Scheme
参考文献
Hapke, Marko; Kral, Karolin; Spannenberg, Anke
Synthesis, 2011 , # 4 art. no. Z27710SS, p. 642 - 652
871-84-1
+
32721-21-4
1-碘-2-甲氧基萘
→
反应条件
755005-65-3
反应条件
piperidine; tetrakis(triphenylphosphine) palladium(0); iodine; zinc(II) chloride T=70°C; 6 h; Inert atmosphere;
参考文献
Hapke, Marko; Kral, Karolin; Fischer, Christine; Spannenberg, Anke; Gutnov, Andrey; Redkin, Dmitry; Heller, Barbara
Journal of Organic Chemistry, 2010 , vol. 75, # 12 p. 3993 - 4003
32721-21-4
1-碘-2-甲氧基萘
+
98-80-6
→
反应条件
75907-52-7
反应条件
1,1'-bis(di-tert-butylphosphino)ferrocene palladium dichloride; triethylamine in water T=20°C; Suzuki-Miyaura reaction; 9 h; Inert atmosphereMicellar solution;
参考文献
Lipshutz, Bruce H.; Petersen, Tue B.; Abela, Alexander R.
Organic Letters, 2008 , vol. 10, # 7 p. 1333 - 1336
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