4,4'-二氨基-3,3'-二硝基二苯基醚合成路线 （共 17 条）
反应条件
water; sodium hydroxide T=100°C;
参考文献
Imoto, Mitsutaka; Takeda, Motonori; Tamaki, Akihiro; Taniguchi, Hisaji; Mizuno, Kazuhiko
Organic Preparations and Procedures International, 2010 , vol. 42, # 2 p. 161 - 167
反应条件
bromine; silver nitrate; triphenylphosphine in acetonitrile T=20°C; 0.0833333 h;
参考文献
Iranpoor, Nasser; Firouzabadi, Habib; Nowrouzi, Najmeh; Firouzabadi, Dena
Tetrahedron Letters, 2006 , vol. 47, # 38 p. 6879 - 6881
反应条件
1: 94 percent / HNO3; AcOH; Ac2O / urea / 50 - 60 °C 2: 96 percent / aq. NaOH / propan-2-ol / 80 °C View Scheme
参考文献
Russian Journal of General Chemistry, , vol. 75, # 10 p. 1509 - 1513
反应条件
1: 92 percent / K2CO3 / dimethylformamide / 10 h / 145 - 150 °C 2: 95 percent / NH2NH2; FeCl3; activated charcoal / dioxane 3: 93 percent / chlorobenzene / 2 h / 90 - 95 °C 4: 94 percent / HNO3; AcOH; Ac2O / urea / 50 - 60 °C 5: 96 percent / aq. NaOH / propan-2-ol / 80 °C View Scheme
参考文献
Russian Journal of General Chemistry, , vol. 75, # 10 p. 1509 - 1513
反应条件
1: 95 percent / NH2NH2; FeCl3; activated charcoal / dioxane 2: 93 percent / chlorobenzene / 2 h / 90 - 95 °C 3: 94 percent / HNO3; AcOH; Ac2O / urea / 50 - 60 °C 4: 96 percent / aq. NaOH / propan-2-ol / 80 °C View Scheme
参考文献
Russian Journal of General Chemistry, , vol. 75, # 10 p. 1509 - 1513
反应条件
1: 94 percent / HNO3; AcOH; Ac2O / urea / 50 - 60 °C 2: 96 percent / aq. NaOH / propan-2-ol / 80 °C View Scheme
参考文献
Russian Journal of General Chemistry, , vol. 75, # 10 p. 1509 - 1513
反应条件
1: 80 percent / NH2NH2; FeCl3; activated charcoal 2: 94 percent / HNO3; AcOH; Ac2O / urea / 50 - 60 °C 3: 96 percent / aq. NaOH / propan-2-ol / 80 °C View Scheme
参考文献
Russian Journal of General Chemistry, , vol. 75, # 10 p. 1509 - 1513
反应条件
1: 93 percent / K2CO3 / dimethylformamide / 10 h / 145 - 150 °C 2: 80 percent / NH2NH2; FeCl3; activated charcoal 3: 94 percent / HNO3; AcOH; Ac2O / urea / 50 - 60 °C 4: 96 percent / aq. NaOH / propan-2-ol / 80 °C View Scheme
参考文献
Russian Journal of General Chemistry, , vol. 75, # 10 p. 1509 - 1513
反应条件
1: 80 percent / NH2NH2; FeCl3; activated charcoal 2: 94 percent / HNO3; AcOH; Ac2O / urea / 50 - 60 °C 3: 96 percent / aq. NaOH / propan-2-ol / 80 °C View Scheme
参考文献
Russian Journal of General Chemistry, , vol. 75, # 10 p. 1509 - 1513
反应条件
1: 84 percent / K2CO3 2: 80 percent / NH2NH2; FeCl3; activated charcoal 3: 94 percent / HNO3; AcOH; Ac2O / urea / 50 - 60 °C 4: 96 percent / aq. NaOH / propan-2-ol / 80 °C View Scheme
参考文献
Russian Journal of General Chemistry, , vol. 75, # 10 p. 1509 - 1513
