2-甲氧基蒽-9,10-二酮合成路线 （共 50 条）
反应条件
chromium(VI) oxide; water; acetic acid
参考文献
Blicke; Weinkauff
Journal of the American Chemical Society, 1932 , vol. 54, p. 1446,1451
反应条件
lead(IV) acetate in dichloromethane T=-50°C;
参考文献
Kuzuya, Masayuki; Miyake, Fumio; Okuda, Takachiyo
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1984 , # 9 p. 1471 - 1478
反应条件
1: 1) NBS / 1) CCl4, 2) DMSO 2: 1) LDA, 2) LDA / 1) THF, -70 deg C, 10 min., 2) THF, -40 deg C, 10 min 3: 90 percent / 10percent aq. NaOH, 30percent aq. H2O2 / ethanol / a) 5 h, 75 deg C, b) 12 h, room temp. View Scheme
参考文献
Bhawal, Baburao M.; Khanapure, Subhash P.; Zhang, Hongming; Biehl, Edward R.
Journal of Organic Chemistry, 1991 , vol. 56, # 8 p. 2846 - 2849
反应条件
1: 1) LDA, 2) LDA / 1) THF, -70 deg C, 10 min., 2) THF, -40 deg C, 10 min 2: 90 percent / 10percent aq. NaOH, 30percent aq. H2O2 / ethanol / a) 5 h, 75 deg C, b) 12 h, room temp. View Scheme
参考文献
Bhawal, Baburao M.; Khanapure, Subhash P.; Zhang, Hongming; Biehl, Edward R.
Journal of Organic Chemistry, 1991 , vol. 56, # 8 p. 2846 - 2849
反应条件
1: potassium tert-butylate / ethanol / 1 h 2: copper diacetate; silver carbonate; oxygen / N,N-dimethyl-formamide / 36 h / 140 °C / 760.05 Torr View Scheme
参考文献
Bhadra, Sukalyan; Dzik, Wojciech I.; Goossen, Lukas J.
Angewandte Chemie - International Edition, 2013 , vol. 52, # 10 p. 2959 - 2962
Angew. Chem., 2013 , vol. 125, # 10 p. 3031 - 3035,4
反应条件
1: AlCl3, aluminium chloride; sodium chloride / 0.75 h / 165 - 170 °C 2: sodium hydride / tert-butyl methyl ether; N,N-dimethyl-formamide / 20 h / 20 °C View Scheme
参考文献
Saha, Koushik; Lam, Kok Wai; Abas, Faridah; Sazali Hamzah; Stanslas, Johnson; Hui, Lim Siang; Lajis, Nordin H.
Medicinal Chemistry Research, 2013 , vol. 22, # 5 p. 2093 - 2104
反应条件
alkali hydroxide T=130°C; unter Druck;
参考文献
Bayer and Co.
Patent: DE166748 ;
参考文献
Sato et al.
Journal of Biochemistry (Tokyo, Japan), 1956 , vol. 443, p. 21,23
参考文献
Scholl; Eberle
Monatshefte fuer Chemie, 1911 , vol. 32, p. 1038
反应条件
potassium hydroxide; air
参考文献
Schemjakin et al.
Zhurnal Obshchei Khimii, 1959 , vol. 29, p. 1831,1837;engl.Ausg.S.1802,1807
