2-甲氧基蒽-9,10-二酮合成路线 （共 50 条）
反应条件
aluminium trichloride
参考文献
Sartori, Giovanni; Casnati, Giuseppe; Bigi, Franca; Robles, Pasquale
Tetrahedron Letters, 1987 , vol. 28, # 14 p. 1533 - 1536
参考文献
Woroshzow; Aleksandrow
Zhurnal Obshchei Khimii, 1940 , vol. 10, p. 869,877,878
Chem. Zentralbl., 1940 , vol. 111, # II p. 3179
反应条件
1: 1.) n-butyl-lithium / 1.) ether, hexane, reflux, 24 h, 2.) - 78 deg C -> ambient temperature 2: 1.) lithium di-isopropylamide, 2.) air / 1.) THF, -70 - -60 deg C, 2.) THF, 20 deg C, 22 h View Scheme
参考文献
Dodsworth, David J.; Calcagno, Maria-Pia; Ehrmann, E. Ursula; Devadas, Bhatt; Sammes, Peter G.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 2120 - 2124
反应条件
2: ethanolic KOH; air View Scheme
参考文献
Schemjakin et al.
Zhurnal Obshchei Khimii, 1959 , vol. 29, p. 1831,1837;engl.Ausg.S.1802,1807
反应条件
1: acetic acid; aqueous HCl 2: FeCl3; acetic acid; ethanol View Scheme
参考文献
Attree; Perkin
Journal of the Chemical Society, 1931 , p. 144,152
反应条件
methanol; potassium ethanolate
参考文献
Kaufler
Chemische Berichte, 1904 , vol. 37, p. 63
反应条件
ethanol; iron(III) chloride; acetic acid
参考文献
Attree; Perkin
Journal of the Chemical Society, 1931 , p. 144,152
反应条件
air; lithium diisopropyl amide 1.) THF, -70 - -60 deg C, 2.) THF, 20 deg C, 22 h; Yield given. Multistep reaction;
参考文献
Dodsworth, David J.; Calcagno, Maria-Pia; Ehrmann, E. Ursula; Devadas, Bhatt; Sammes, Peter G.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 2120 - 2124
反应条件
air; lithium diisopropyl amide 1.) THF, -70 - -60 deg C, 2.) THF, 20 deg C, 22 h; Yield given. Multistep reaction;
参考文献
Dodsworth, David J.; Calcagno, Maria-Pia; Ehrmann, E. Ursula; Devadas, Bhatt; Sammes, Peter G.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 2120 - 2124
参考文献
Kaufler
Chemische Berichte, 1904 , vol. 37, p. 63
