1-溴-3-氯-2-氟丙烷合成路线 （共 12 条）
反应条件
N-bromosuccinmide; hydrogen fluoride in tetrahydrofuran 1.) dry ice-isopropyl alcohol bath, 30 min, 2.) -10 deg C, 1 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Kunshenko, B. V.; Mokhamed, Nagib Mukhtar; Omarov, V. O.; Muratov, N. N.; Yagupol'skii, L. M.
Journal of Organic Chemistry USSR (English Translation), 1992 , vol. 28, # 4.1 p. 511 - 518
Zhurnal Organicheskoi Khimii, 1992 , vol. 28, # 4 p. 672 - 680
反应条件
bromine trifluoride in various solvent(s) T=10 - 20°C; 4 h;
参考文献
Boguslavskaya, L. S.; Chuvatkin, N. N.; Panteleeva, I. Yu.; Ternovskoi, L. A.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, # 5 p. 814 - 820
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 5 p. 938 - 945
反应条件
bromine trifluoride; bromine in 1,2,2-trifluoro-trichloroethane T=10 - 20°C;
参考文献
Boguslavskaya, L. S.; Chuvatkin, N. N.; Kartashov, A. V.; Ternovskoi, L. A.
Journal of Organic Chemistry USSR (English Translation), 1987 , vol. 23, p. 230 - 236
Zhurnal Organicheskoi Khimii, 1987 , vol. 23, # 2 p. 262 - 269
反应条件
bromine trifluoride in 1,2,2-trifluoro-trichloroethane T=10 - 20°C;
参考文献
Chuvatkin, N. N.; Kartashov, A. V.; Morozova, T. V.; Boguslavskaya, L. S.
Journal of Organic Chemistry USSR (English Translation), 1987 , vol. 23, # 2 p. 237 - 242
Zhurnal Organicheskoi Khimii, 1987 , vol. 23, # 2 p. 269 - 274
反应条件
bromine trifluoride in 1,2,2-trifluoro-trichloroethane 1 h;
参考文献
Boguslavskaya, L. S.; Chuvatkin, N.; Morozova, T. V.; Panteleeva, I. Yu.; Kartashov, A. V.; Sineokov, A. P.
Journal of Organic Chemistry USSR (English Translation), 1987 , p. 1060 - 1064
Zhurnal Organicheskoi Khimii, 1987 , vol. 23, # 6 p. 1173 - 1177
反应条件
hydrogen fluoride; hexachloromelamine T=-15 - 0°C; 4 h; Yield given. Yields of byproduct given;
参考文献
Chuvatkin, N. N.; Morozova, T. V.; Boguslavskaya, L. S.
Journal of Organic Chemistry USSR (English Translation), 1983 , p. 990 - 991
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 5 p. 1107 - 1109
反应条件
fluoro chloride in chloroform in the dark; Yield given. Yields of byproduct given;
参考文献
Boguslavskaya, L. S.; Chuvatkin, N. N.; Panteleeva, I. Yu.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, # 10 p. 1832 - 1842
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 10 p. 2082 - 2094
反应条件
hydrogenchloride; hydrogen fluoride
参考文献
Boguslavskaya,L.S.; Bulovyatova,A.B.
Zhurnal Organicheskoi Khimii, 1971 , vol. 7, p. 443 - 447,447 - 451
反应条件
bromine trifluoride in 1,2,2-trifluoro-trichloroethane T=20 - 25°C; Product distribution;
参考文献
Kartashov, A. V.; Chuvatkin, N. N.; Kurskii, Yu. A.; Boguslavskaya, L. S.
Journal of Organic Chemistry USSR (English Translation), 1988 , vol. 24, # 12 p. 2279 - 2284
Zhurnal Organicheskoi Khimii, 1988 , vol. 24, # 12 p. 2525 - 2531
反应条件
bromine trifluoride; hydrogen fluoride T=-20°C; 0.5 h; Product distribution;
参考文献
Kartashov, A. V.; Chuvatkin, N. N.; Kurskii, Yu. A.; Boguslavskaya, L. S.
Journal of Organic Chemistry USSR (English Translation), 1988 , vol. 24, # 12 p. 2279 - 2284
Zhurnal Organicheskoi Khimii, 1988 , vol. 24, # 12 p. 2525 - 2531
