2-异氰基-3-甲基丁酸叔丁酯合成路线 （共 3 条）
反应条件
triethylamine; trichlorophosphate in tetrahydrofuran T=-78 - 0°C; 1 h;
参考文献
Monge, David; Jensen, Kim L.; Marin, Irene; Jorgensen, Karl Anker
Organic Letters, 2011 , vol. 13, # 2 p. 328 - 331
反应条件
1: acetic anhydride / 2 h / 0 - 20 °C 2: triethylamine; trichlorophosphate / tetrahydrofuran / 1 h / -78 - 0 °C View Scheme
参考文献
Monge, David; Jensen, Kim L.; Marin, Irene; Jorgensen, Karl Anker
Organic Letters, 2011 , vol. 13, # 2 p. 328 - 331
反应条件
(i) KOtBu, THF, (ii) /BRN= 1098244/; Multistep reaction;
参考文献
Schoellkopf,U. et al.
Chemische Berichte, 1975 , vol. 108, p. 1580 - 1592
Full Text Show Details
Schoellkopf,U. et al.
Angewandte Chemie, 1971 , vol. 83, p. 357 - 358
