(3E)-5-甲基己-1,3-二烯合成路线 （共 15 条）
反应条件
T=650°C; P=0.01 Torr;
参考文献
Bloch, R.; Abecassis, J.; Hassan, D.
Canadian Journal of Chemistry, 1984 , vol. 62, p. 2019 - 2024
参考文献
Maciagiewicz; Dybowski; Skowronska
Polish Journal of Chemistry, 2005 , vol. 79, # 3 p. 515 - 523
反应条件
1: NaI; triethylamine / acetonitrile 2: CH2Cl2 / 1 h / 20 °C 3: 71 percent / NaBH4 / diethyl ether; methanol / 1 h / 10 - 20 °C 4: 70 percent / triphenylphosphine View Scheme
参考文献
Maciagiewicz; Dybowski; Skowronska
Tetrahedron Letters, 1999 , vol. 40, # 19 p. 3791 - 3794
反应条件
1: CH2Cl2 / 1 h / 20 °C 2: 71 percent / NaBH4 / diethyl ether; methanol / 1 h / 10 - 20 °C 3: 70 percent / triphenylphosphine View Scheme
参考文献
Maciagiewicz; Dybowski; Skowronska
Tetrahedron Letters, 1999 , vol. 40, # 19 p. 3791 - 3794
反应条件
1: 71 percent / NaBH4 / diethyl ether; methanol / 1 h / 10 - 20 °C 2: 70 percent / triphenylphosphine View Scheme
参考文献
Maciagiewicz; Dybowski; Skowronska
Tetrahedron Letters, 1999 , vol. 40, # 19 p. 3791 - 3794
反应条件
water; hydrogen bromide Dehydration;
参考文献
Viktorov; Zubritskii
Russian Journal of Organic Chemistry, 1999 , vol. 35, # 12 p. 1755 - 1765
参考文献
Gassman,P.G. et al.
Journal of the American Chemical Society, 1972 , vol. 94, p. 7741 - 7748
参考文献
Nativi, Cristina; Ricci, Alfredo; Taddei, Maurizio
Tetrahedron Letters, 1987 , vol. 28, # 24 p. 2751 - 2752
反应条件
1: 1.) CF3SO3H, 2.) ammonium chloride / 1.) THF, 0 deg C, 1 min 2: H(1+) View Scheme
参考文献
Nativi, Cristina; Ricci, Alfredo; Taddei, Maurizio
Tetrahedron Letters, 1987 , vol. 28, # 24 p. 2751 - 2752
反应条件
sodium hydride; dimethyl sulfoxide 1.) room temp., 0.5 h, 2.) room temp. 1 h; Yield given. Multistep reaction;
参考文献
Kuwano; Ohshima; Eto
Agricultural and Biological Chemistry, 1980 , vol. 44, # 2 p. 383 - 386
