1,1,3,3-四甲基二硅氧烷合成路线 (共 158 条)
反应条件
72 h; Ambient temperature;
参考文献
Voronkov, M.G.; Basenko, S.V.; Gebel, I.A.; Vitkovskii, V.Yu.; Mirskov, R.G.
Journal of Organometallic Chemistry, 1992 , vol. 433, # 1-2 p. 1 - 9
反应条件
72 h; Ambient temperature;
参考文献
Voronkov, M.G.; Basenko, S.V.; Gebel, I.A.; Vitkovskii, V.Yu.; Mirskov, R.G.
Journal of Organometallic Chemistry, 1992 , vol. 433, # 1-2 p. 1 - 9
反应条件
72 h; Ambient temperature;
参考文献
Voronkov, M.G.; Basenko, S.V.; Gebel, I.A.; Vitkovskii, V.Yu.; Mirskov, R.G.
Journal of Organometallic Chemistry, 1992 , vol. 433, # 1-2 p. 1 - 9
反应条件
72 h; Ambient temperature;
参考文献
Voronkov, M.G.; Basenko, S.V.; Gebel, I.A.; Vitkovskii, V.Yu.; Mirskov, R.G.
Journal of Organometallic Chemistry, 1992 , vol. 433, # 1-2 p. 1 - 9
反应条件
NaHF2
T=120°C; 0.05 h; other times, other temp.; Product distribution;
参考文献
Filippov, A. M.; Bochkarev, V. N.
J. Gen. Chem. USSR (Engl. Transl.), 1990 , vol. 60, # 4.2 p. 865 - 867,760 - 761
参考文献
Emeleus; Onyszchuk
Journal of the Chemical Society, 1958 , p. 604,606
反应条件
in toluene
dispersing GaCl3 in toluene at 0°C under dry N2; addn. of siloxane during 1h with stirring; stirring for 12h at ambient temp.; large amount of insol. and unvolatile material;
参考文献
Bissinger, Peter; Mikulcik, Patrizia; Riede, Juergen; Schier, Annette; Schmidbaur, Hubert
Journal of Organometallic Chemistry, 1993 , vol. 446, # 1.2 p. 37 - 43
反应条件
di-μ-chloro-bis(η4-1,5-cyclooctadiene)diiridium; biphenyl in deuterated toluene
T=40°C; 3 h; Sealed tubeInert atmosphere;
参考文献
Igarashi, Masayasu; Matsumoto, Tomohiro; Kobayashi, Toshiaki; Sato, Kazuhiko; Ando, Wataru; Shimada, Shigeru; Hara, Masanao; Uchida, Hiroshi
Journal of Organometallic Chemistry, 2014 , vol. 752, p. 141 - 146
参考文献
De Vekki; Skvortsov
Russian Journal of General Chemistry, 2009 , vol. 79, # 4 p. 762 - 777
反应条件
karstedt's catalyst
T=60 - 85°C; 16.5 h; Heating / reflux;
参考文献
Rajaraman, Suresh K.; Leatherman, Mark D.; Rojas-Wahl, Roy U.; Razzano, John S.
Patent: US2005/265942 A1, 2005 ;
Location in patent: Page/Page column 6 ;