(4-溴苯基)(环己基)甲酮合成路线 （共 8 条）
反应条件
bis-triphenylphosphine-palladium(II) chloride; potassium carbonate in water; benzene T=20°C; P=34202.3 Torr; 16 h; AutoclaveIrradiation;
参考文献
Sumino, Shuhei; Ui, Takahito; Ryu, Ilhyong
Organic Letters, 2013 , vol. 15, # 12 p. 3142 - 3145
反应条件
manganese(IV) oxide in dichloromethane T=20°C;
参考文献
WO2012/175520 A1, ;
Page/Page column 113 ;
反应条件
AlCl3, aluminium chloride in neat (no solvent) T=20°C; Friedel-Crafts Acylation; Inert atmosphere;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 23, # 24 p. 6629 - 6635
反应条件
iron tribromide in toluene T=110°C; Wagner-Meerwein Rearrangement; 20 h; Sealed tubeSchlenk techniqueInert atmosphere; chemoselective reaction;
参考文献
Gutierrez-Bonet, Alvaro; Flores-Gaspar, Areli; Martin, Ruben
Journal of the American Chemical Society, 2013 , vol. 135, # 34 p. 12576 - 12579
反应条件
1: diethyl ether; tetrahydrofuran / 1 h / Cooling with methanol ice 2: manganese(IV) oxide / dichloromethane / 20 °C View Scheme
反应条件
1: diethyl ether; tetrahydrofuran / 1 h / Cooling with methanol ice 2: manganese(IV) oxide / dichloromethane / 20 °C View Scheme
反应条件
1: sodium hexamethyldisilazane / |Inert atmosphere; |Schlenk technique 2: diisobutylaluminium hydride / |Inert atmosphere; |Schlenk technique 3: iron tribromide / toluene / 20 h / 110 °C / |Sealed tube; |Schlenk technique; |Inert atmosphere View Scheme
参考文献
Journal of the American Chemical Society, , vol. 135, # 34 p. 12576 - 12579
反应条件
1: diisobutylaluminium hydride / |Inert atmosphere; |Schlenk technique 2: iron tribromide / toluene / 20 h / 110 °C / |Sealed tube; |Schlenk technique; |Inert atmosphere View Scheme
参考文献
Journal of the American Chemical Society, , vol. 135, # 34 p. 12576 - 12579
